Preparation method of novel wool fabric milling detergent
A cleaning agent and fat technology, which is applied in the field of preparation of a new type of woollen denim cleaning agent, can solve the problems of poor biodegradability, rigid fabrics, serious environmental pollution, etc. Excellent wash performance
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[0020] 1) Preparation of hydroxymethylacrylic acid, maleic anhydride and acrylamide copolymer: a. Add maleic anhydride (1.0mol) and water to a 1000ml four-necked flask equipped with a thermometer, reflux condenser, and double dropping funnel (500ml), heat up to 50~80°C, stir to dissolve, add 20~30% sodium hydroxide solution to adjust the pH to 5.5~7.0, and obtain liquid a; b. Weigh hydroxyacrylic acid (2.3mol), sodium persulfate ( 0.05mol), dissolved in 100ml water to obtain liquid b; c, weigh acrylamide (0.5mol); d, double drop b and c into liquid a at the same time, control the dropping temperature at 80~110°C, drop The time is 3~6 hours, the drop is completed, and the reaction is carried out under reflux for 10~16 hours. After the reaction is completed, the temperature is lowered to 50°C, and a yellow viscous polymer product is obtained.
[0021] 2) Compounding of woolen shrinkage cleaning agent: Add 9g of fatty alcohol polyoxyethylene ether-15, 10g of fatty alcohol polyoxy...
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