Preparation method for grain extracting solution
A technology of extracting liquid and grain, which is applied in the field of preparation of grain extract, which can solve the problems of difficult to restore grain aroma, thin aroma, sensory impact, etc., and achieve the effect of natural and pure aroma, preventing oxidation, and strong grain aroma
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Embodiment 1
[0029] A kind of preparation method of grain extract, its operation steps are as follows:
[0030] Weigh 10 kg of barley with shells, remove impurities and screen and bake. The feed temperature of the baking furnace was set at 180°C, the discharge temperature was set at 235°C, and the heating rate was set at 2°C / min. Immediately after the baking is finished, the air is blown to cool, and the cooling rate is 80°C / min. Pulverize after being cooled to room temperature, sieve with 40 mesh standard sieves, control the barley particle after pulverizing to pass 40 mesh sieves and account for 2%. According to the ratio of material to liquid of 1:10g / L, mix the pulverized barley raw material with ethanol solution with a volume concentration of 85%, and extract for 90min under a nitrogen atmosphere, the extraction temperature is 100°C, and the nitrogen flow rate is 1L / min, recover condensate. Concentrate the condensate in vacuum, the vacuum degree is -0.1Mpa, the time is 30min, the ...
Embodiment 2
[0032] A kind of preparation method of grain extract, its operation steps are as follows:
[0033] Weigh 10kg of barley, remove impurities and screen and roast. The feed temperature of the baking furnace is set to 150°C, the discharge temperature is set to 200°C, and the heating rate is set to 3°C / min. Immediately after the baking is finished, the air is blown to cool, and the cooling rate is 50°C / min. Pulverize after being cooled to room temperature, sieve with 40 mesh standard sieves, control the barley particle after pulverizing to pass 40 mesh sieves and account for 3%. According to the material-liquid ratio of 1:25g / L, mix the pulverized barley raw material with the ethanol solution with a volume concentration of 60%, and extract for 60min under nitrogen atmosphere, the extraction temperature is 120°C, and the nitrogen flow rate is 1.5 L / min, recover condensate. Concentrate the condensate in vacuum, the vacuum degree is -0.1Mpa, the time is 15min, the temperature is 45...
Embodiment 3
[0035] A kind of preparation method of grain extract, its operation steps are as follows:
[0036] Weigh 10kg black beans, remove impurities and screen and roast. The feed temperature of the baking furnace was set at 200°C, the discharge temperature was set at 235°C, and the heating rate was set at 1°C / min. Immediately after the baking is finished, the air is blown to cool, and the cooling rate is 65° C. / min. Pulverize after being cooled to room temperature, sieve with 40 mesh standard sieves, control the barley particle after pulverizing to pass 40 mesh sieves and account for 5%. According to the ratio of solid-liquid ratio of 1:40g / L, mix the pulverized barley raw material with ethanol solution with a volume concentration of 30%, and extract for 30min under nitrogen atmosphere, the extraction temperature is 150°C, and the nitrogen flow rate is 2.0 L / min, recover condensate. Concentrate the condensate in vacuum, the vacuum degree is -0.1Mpa, the time is 30min, the temperat...
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