Production process for complete set of general asphalt carbon fiber
A production process and general-purpose technology, applied to the chemical characteristics of fibers, textiles and papermaking, etc., can solve the problems of low product performance, lack of transformation funds, and no industrial production capacity, etc., to achieve low industrialization costs, simple process conditions, The effect of strong industrialization operability
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Embodiment 1
[0016] A production process of a complete set of general-grade pitch carbon fiber, comprising the following steps:
[0017] (1) Add heavy aromatic components with 5% carbon residue and 0.015% ash content to the 1# reactor, control the temperature of the reactor to 300°C, and feed air into the reactor, and the gas volume required for raw materials is 0.15m 3 / h / kg, stirring and reacting for 16 hours to obtain oxidized asphalt with a softening point of 180°C, and then pump the oxidized asphalt into the continuous reactor through a high-temperature delivery pump. The temperature of the continuous reactor is 370°C, and the continuous reactor is pumped Vacuum, the vacuum degree is -0.098MPa, the oxidized asphalt is reacted in the continuous reactor for 2 hours to make thermal condensation asphalt, and then the thermal condensation asphalt in the continuous reactor is transported to the continuous granulation equipment through the metering pump, and prepared according to the conventi...
Embodiment 2
[0023] A production process of a complete set of general-grade pitch carbon fiber, comprising the following steps:
[0024] (1) Add the heavy components of aromatics with 15% carbon residue, 0.01% ash, and a softening point of 70°C to the 1# reactor, control the temperature of the reactor to 310°C, and feed air into the reactor, The required gas volume is 0.12m 3 / h / kg, stirring and reacting for 12 hours to obtain oxidized asphalt with a softening point of 190°C, and then pump the oxidized asphalt into the continuous reactor through a high-temperature delivery pump. The temperature of the continuous reactor is 380°C, and the continuous reactor is pumped Vacuum, the vacuum degree is -0.098MPa, the oxidized asphalt is reacted in the continuous reactor for 1.5h, and the heat-condensed asphalt is made, and then the heat-condensed asphalt in the continuous reactor is transported to the continuous granulation equipment through the metering pump, and prepared according to the convent...
Embodiment 3
[0030] A production process of a complete set of general-grade pitch carbon fiber, comprising the following steps:
[0031] (1) Add heavy aromatic components with 20% carbon residue, 0.01% ash, and a softening point of 90°C to the 1# reactor, control the temperature of the reactor to 315°C, and feed air into the reactor. The required gas volume is 0.12m 3 / h / kg, stirring and reacting for 14 hours to obtain oxidized asphalt with a softening point of 200°C, and then pump the oxidized asphalt into the continuous reactor through a high-temperature delivery pump. The temperature of the continuous reactor is 380°C, and the continuous reactor is pumped Vacuum, the vacuum degree is -0.098MPa, the oxidized asphalt is reacted in the continuous reactor for 2 hours to make thermal condensation asphalt, and then the thermal condensation asphalt in the continuous reactor is transported to the continuous granulation equipment through the metering pump, and prepared according to the conventio...
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