Preparation method of super-hydrophobic polyester textile

A textile and superhydrophobic technology, applied in textiles and papermaking, fiber treatment, fiber types, etc., can solve problems such as poor fiber affinity, poor durability of superhydrophobic fabrics, and solvent pollution

Active Publication Date: 2013-03-13
南京哈昵特户外用品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Most of these materials are inorganic nanoparticles, which have poor affinity with fibers, so the durability of the prepared superhydrophobic fabric is not good.
In addition, when performing low surface energy treatment on substrates, most methods require the use of so

Method used

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  • Preparation method of super-hydrophobic polyester textile
  • Preparation method of super-hydrophobic polyester textile
  • Preparation method of super-hydrophobic polyester textile

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Step 1: Treat polyester fabric with alkali: first soak the polyester fabric in warm water at a temperature of 40°C, then immerse the fabric in a bath ratio of 40:1, a concentration of sodium hydroxide of 5g / L, and a concentration of accelerator 1227 of 2g / L of finishing solution, heated at 90°C for 50min, and finally took out the fabric, fully washed it with deionized water, and dried it at 80°C to obtain an alkali-treated polyester fabric.

[0031] Step 2: In the absence of solvent, place the alkali-treated polyester fabric in a dyeing vat, add 30% heptadecafluorodecyltrimethoxysilane to the fabric weight, seal it, treat it at 130°C for 1 hour, and take out the fabric Bake at 70°C for 90min. The surface contact angle of the obtained fabric is 159.6 °, and after the obtained fabric is worn 2000 times on the AATCC color fastness tester against rubbing, its contact angle with water droplets is 155.5 °, and the soap powder boiling water with a solubility of 5g / L After me...

Embodiment 2

[0033] Step 1: Treat polyester fabric with alkali: first soak the polyester fabric in warm water, then immerse the fabric in a finishing solution with a bath ratio of 40:1, a sodium hydroxide concentration of 5g / L, and an accelerator 1227 concentration of 2g / L , heated at 90°C for 50min, and finally the fabric was taken out, fully washed with deionized water, and dried at 80°C to obtain an alkali-treated polyester fabric.

[0034] Step 2: In the absence of solvent, place the alkali-treated polyester fabric in a dye vat, add 30% hexadecyltrimethoxysilane to the weight of the fabric, seal it, treat it at 150°C for 0.5h, and take out the fabric Bake at 100°C for 60 minutes. The surface contact angle of the obtained fabric is 161.2 °, and after the obtained fabric is worn 2000 times on the AATCC color fastness tester against rubbing, its contact angle with water droplets is 153.2 °, and the soap powder boiling water with a solubility of 5g / L After medium cooking for 180min, the c...

Embodiment 3

[0036] Step 1: Treatment of polyester fabric with alkali: first soak the polyester fabric in warm water, then immerse the fabric in a finishing process with a bath ratio of 40:1, a sodium hydroxide concentration of 18g / L, and an accelerator 1227 concentration of 1.5g / L solution, heated at 90°C for 50min, and finally the fabric was taken out, fully washed with deionized water, and dried at 80°C to obtain an alkali-treated polyester fabric.

[0037] Step 2: In the absence of solvent, place the alkali-treated polyester fabric in a dyeing vat, add 10% heptadecafluorodecyltrimethoxysilane to the weight of the fabric, seal it, treat it at 100°C for 1.5h, and take out the fabric Bake at 150°C for 30min. The surface contact angle of the obtained fabric is 163.8 °, and after the obtained fabric is worn 2000 times on the AATCC color fastness tester against rubbing, its contact angle with water droplets is 156.9 °, and the soap powder boiling water with a solubility of 5g / L After medium...

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Abstract

The invention provides a preparation method of a super-hydrophobic polyester textile. The method includes: first conducting alkali treatment on a polyester fabric so as to make fiber surfaces etched by alkali and generate uneven pits, thus improving fiber surface roughness; and then putting the fabric into a dye vat, adding a low-surface energy material, conducting sealing, and performing treatment at 80-150DEG C. The polyester textile prepared by the method has a surface water-drop static contact angle greater than 150 degrees. In the invention, no solvent is employed when low-surface energy material treatment is conducted on the fabric, thus the method is environment-friendly. In addition, the method can make the low-surface energy material go deep into the fibers, so that the prepared super-hydrophobic polyester textile has long-lasting super-hydrophobicity.

Description

【Technical field】 [0001] The invention relates to a preparation method of functional textiles, in particular to a preparation method of superhydrophobic polyester textiles. 【Background technique】 [0002] Superhydrophobic textiles have special wettability, that is, the contact angle of water droplets on the surface of the fabric is greater than 150°, and it is easy to roll on its surface. The water droplets will take away the dirt on the surface during the rolling process, which is the so-called "lotus leaf self-cleaning effect". At the same time, the super-hydrophobic property enables the product to achieve "not wet after rain, retractable at any time", and also avoids the impregnation, degradation and aging of the fiber matrix by water, thereby prolonging the service life of the fabric. Superhydrophobic textiles are widely used in industrial production, medical treatment, military products and daily life. [0003] There are two key technologies for preparing a super-hydr...

Claims

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Application Information

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IPC IPC(8): D06M11/38D06M13/513D06M101/32
Inventor 薛朝华张平贾顺田马建中
Owner 南京哈昵特户外用品有限公司
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