A method for preparing Y-modified CoalNI coating on Ni-based superalloy by adopting embedding infiltration process
A high-temperature alloy and embedding infiltration technology, which is applied in the direction of coating, metal material coating process, solid-state diffusion coating, etc., can solve the problems of reducing the oxidation resistance and thermal corrosion resistance of high-temperature alloys
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[0029] The present invention relates to a method for preparing a Y-modified CoAlNi coating on a Ni-based superalloy by adopting an embedding and infiltration process. The coating preparation method has the following steps:
[0030] The first step: pretreatment of the substrate
[0031] (A) The surface of the Ni-based superalloy was polished with 800# SiC water abrasive paper to obtain the first sample;
[0032] The surface roughness of the first sample is Ra=1.6;
[0033] (B) After putting the first sample into absolute ethanol for 10-15 minutes of ultrasonic cleaning, the second sample was obtained;
[0034] The second step: preparation of embedding seepage material
[0035] Prepare 100g of embedding material by 6-8g of Al powder with a particle size of 100 mesh, 15-25g of Co powder with a particle size of 100 mesh, and 1-3g of Y with a particle size of 100 mesh 2 o 3 Powder, 3~5g NH with a particle size of 100 mesh 4 Cl powder, 3-5g NH with a particle size of 100 mesh ...
Embodiment 1
[0046] The substrate is Ni-6.2Co-8.9Cr-7.0W-6.1Al-3.8Ta-2.0Mo-1.5Hf-1.0Ti (brand DZ125).
[0047] The first step: pretreatment of the substrate
[0048] (A) The surface of the Ni-based superalloy is polished with 800# SiC water-grinding paper to prepare the first sample;
[0049] The surface roughness of the first sample is Ra=1.6;
[0050] (B) After placing the first sample in absolute ethanol for ultrasonic cleaning for 10 to 15 minutes, the second sample is obtained;
[0051] The second step: making the embedding material
[0052] 100g of embedded infiltration material is prepared from 7.6g of Al powder with a particle size of 100 mesh, 20g of Co powder with a particle size of 100 mesh, and 2g of Y with a particle size of 100 mesh. 2 O 3 Powder, 4g particle size is 100 mesh NH 4 Cl powder, 4g NH with particle size of 100 mesh 4 I powder and balance particle size are 100 mesh Al 2 O 3 powder composition;
[0053] In the present invention, the added Al 2 O 3 The powd...
Embodiment 2
[0067] The matrix is selected from Ni-10Co-9Cr-12W-5Al-1.5Hf-2Ti (brand DZ22).
[0068] The first step: pretreatment of the substrate
[0069] (A) The surface of the Ni-based superalloy is polished with 800# SiC water-grinding paper to prepare the first sample;
[0070] The surface roughness of the first sample is Ra=1.6;
[0071] (B) After placing the first sample in absolute ethanol for ultrasonic cleaning for 10 to 15 minutes, the second sample is obtained;
[0072] The second step: making the embedding material
[0073] 100g of embedded seepage material is prepared from 6g of Al powder with a particle size of 100 mesh, 15g of Co powder with a particle size of 100 mesh, and 3g of Y with a particle size of 100 mesh. 2 O 3 Powder, 5g particle size is 100 mesh NH 4 Cl powder, 5g particle size of 100 mesh NH 4 I powder and balance particle size are 100 mesh Al 2 O 3 powder composition;
[0074] In the present invention, the added Al 2 O 3 The powder does not partic...
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