Nylon modified plastic
A modification and plastic technology, applied in the field of nylon modified plastics, can solve the problems of complex synthesis process and pollution, and achieve the effect of wide industrial application prospects.
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Embodiment 1
[0052] Embodiment 1, Preparation of Nylon 56
[0053] The 50-liter enamel salt-forming kettle was vacuumed and filled with nitrogen to replace the air three times, and protected with nitrogen, 30kg of pure water was added to the salt-forming kettle, and then 12.46kg of pentamethylenediamine (purchased from Shandong Kaisai, containing ASTM D6866 standard organic carbon from renewable sources, gas phase normalization method purity 99.56%), start stirring, add 17.64kg of adipic acid (purchased from Liaoning Petrochemical), and then add 6g of antioxidant H10 (Bruggolen H10 German Brug Gehman Company) to prepare nylon saline solution.
[0054] Replace the air in a 100-liter polymerization kettle (K / SY166-2007 type) with nitrogen, and transfer the nylon salt solution to the polymerization kettle. The temperature of the oil bath rises to 230°C. After the pressure in the kettle rises to 1.73Mpa, start to vent. When the temperature in the kettle reaches 265°C, vacuumize to -0.06Mpa (...
Embodiment 2
[0055] Example 2 , the preparation of nylon 56
[0056] Operate in the same manner as in Example 1 except that the amount of pentamethylenediamine added in the adjustment example 1 is 12.39kg. Nylon 56 was obtained with a reduced viscosity of 120ml / g.
Embodiment 3
[0057] Example 3 , the preparation of nylon 56
[0058] Operate in the same manner as in Example 1 except that the amount of pentamethylenediamine added in the adjustment example 1 is 12.54kg. Nylon 56 was prepared with a reduced viscosity of 160ml / g.
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