Novel high-efficiency method for controlling flow-away and degradation of pesticides
A pesticide loss and pesticide technology, applied in the field of pesticides, to achieve the effect of reducing pesticide residues, controlling the degradation of pesticide residues, and being environmentally friendly
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Embodiment 1
[0026] (1) Add 400 mesh colloidal grade attapulgite to tap water to make a suspension with a concentration of 30 g / L, stir at 5000 rpm for 10 minutes, let stand for 20 minutes, discard 1 / 4 volume of the mud in the lower layer, and keep the rest suspension;
[0027] (2) Add ferric chloride to the remaining suspension, keep the concentration of ferric chloride at 2 M, stir and react at 2000 rpm at 30°C for 20 minutes, let it stand for 20 minutes, discard the supernatant, and then add tap water to make it reach the original concentration, and then let it stand to remove the supernatant, and the obtained mud is iron ion-type attapulgite;
[0028] (3) Add 20% mass fraction of polyvinyl alcohol to the mud, stir evenly, and irradiate with a high-energy electron beam with an energy of 10 MeV and a dose of 40 kGy for 10 minutes, and the grafting reaction forms attapulgite-polyvinyl alcohol composite thing;
[0029] (4) Add 20% mass fraction of hydrazine hydrate to the attapulgite-pol...
Embodiment 2
[0035] (1) Add 300 mesh colloidal grade attapulgite to tap water to make a suspension with a concentration of 20 g / L, stir at 6000 rpm for 10 minutes, let stand for 20 minutes, discard 1 / 5 of the volume of the mud in the lower layer, and keep the rest suspension;
[0036] (2) Add ferric chloride to the remaining suspension, keep the concentration of ferric chloride at 1.5 M, stir and react at 2000 rpm at 30°C for 15 minutes, let it stand for 20 minutes, discard the supernatant, and then add tap water to make it reach the original concentration, and then let it stand to remove the supernatant, and the obtained mud is iron ion-type attapulgite;
[0037] (3) Add 15% vinyl alcohol to the mud, stir evenly, and irradiate with a high-energy electron beam with an energy of 10 MeV and a dose of 30 kGy for 5 minutes, and graft reaction forms attapulgite-polyvinyl alcohol composite ;
[0038] (4) Add 15% mass fraction of hydrazine hydrate to the attapulgite-polyvinyl alcohol composite ...
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