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Determination method for ablation residue ratio of heat-insulating material

A heat insulation material and measurement method technology, applied in the direction of weighing by removing certain components, can solve the problems of pressure curve fluctuations, failure to reflect the amount of erosion residue of heat insulation materials or heat insulation layers, and affect the maneuverability of missiles. The method is simple, the control stability is high, and the detection data is accurate.

Inactive Publication Date: 2013-07-17
HUBEI INST OF AEROSPACE CHEMOTECHNOLOGY
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Problems solved by technology

However, this method cannot reflect the amount of ablation residue in the ablation process of the heat insulation material or the heat insulation layer, that is, the amount of residue that is washed away by the high temperature and high speed gas flow during the ablation process. In the prior art, There are no other measures to evaluate this indicator
[0003] However, for the heat insulation materials used in power source devices such as missile servo systems, attitude and orbit control systems in the missile and aerospace fields, it is required that they cannot produce lumps and particles that may block the filter screen or nozzle during work. Shaped shedding residues to avoid fluctuations in the pressure curve of the missile combustion chamber and affect the maneuverability of the missile

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  • Determination method for ablation residue ratio of heat-insulating material
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  • Determination method for ablation residue ratio of heat-insulating material

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Embodiment Construction

[0014] The invention will be further described below in conjunction with three specific embodiments. One case of nitrile rubber insulation layer, EPDM rubber insulation layer and silicone rubber insulation layer was selected to test the ablation residue rate. The specific operation steps and test methods are as follows.

[0015] The first item is the determination of the ablation residue rate of the nitrile rubber insulation layer.

[0016] Step 1, the production, pretreatment and initial quality marking of the test piece before ablation: Take the nitrile rubber insulation material and mold it into a film and ablation piece respectively, let it stand at room temperature for one day, put it in a clean enamel plate, and put it in a 50- Remove volatiles and moisture in an oven at 80°C, weigh the initial mass of the ablation piece before ablation, and mark it as the initial mass before ablation M 1 .

[0017] Step 2. Determination and marking of the carbon residual rate of the ...

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Abstract

The invention relates to a detection method for thermal insulation performance of a rubber heat-insulating material used in the fields of guided missiles and spaceflight, i.e., a determination method for an ablation residue ratio of the heat-insulating material. The determination method comprises the following four steps: making and pretreatment of a to-be-tested member and marking of initial mass; determination and marking of a carbon residue ratio of a film; formation of a to-be-tested ablation member and marking of mass after ablation; and determination of an ablation residue ratio. Through the four steps, determination of the ablation residue ratio of the rubber heat-insulating material is realized; the method can reliably evaluate a residue amount consumed in scouring and exfoliation corrosion by high-temperature high-speed gas flow during the ablation process of the ablation member, greatly guarantees validity, safety and reliability of the heat-insulating material and has the advantages of easiness, accurate detection data, high control stability and good test repeatability.

Description

Technical field [0001] The invention relates to a detection method for the shedding residue of a rubber heat-insulating material used in the missile and aerospace fields, in particular to a method for measuring the ablation residue rate of the heat-insulation material. Background technique [0002] At present, the evaluation of the ablation performance of thermal insulation materials is mainly determined by the oxygen-acetylene ablation test method. By measuring the thickness change, mass change and back wall temperature of the specimen before and after ablation, the linear ablation rate, Parameters such as mass ablation rate and adiabatic index. However, this method cannot reflect the amount of ablation residue in the ablation process of the heat insulation material or the heat insulation layer, that is, the amount of residue that is washed away by the high temperature and high speed gas flow during the ablation process. In the prior art, There is no other measurement meth...

Claims

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Application Information

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IPC IPC(8): G01N5/04
Inventor 陈德宏朱学文凌玲何碧烟张宏雷
Owner HUBEI INST OF AEROSPACE CHEMOTECHNOLOGY
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