Method for preparing self-adhesion rubber asphalt waterproof roll tearing-free film
A technology of bituminous waterproofing membrane and self-adhesive rubber, applied in the direction of coating, etc., can solve the problems of weak bonding, water entanglement, and poor bonding performance of the membrane.
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Embodiment 1
[0028] First, 100 parts of cardanol, 95 parts of formaldehyde aqueous solution (37%) and 2775 parts of polyvinyl alcohol aqueous solution (5%) are added to the reactor, and when the temperature rises to 60°C, an appropriate amount of alkaline solution (5% ), to keep the pH=8.5-9.0, react for 60min. Then add the remaining 95 parts of formaldehyde aqueous solution (37%), and continue to react at 85±2°C for 90 minutes to obtain the membrane stock solution.
[0029] Then neutralize the film stock solution to pH=7.0 first, then dilute to 5%, and apply it on the surface of the freshly formed self-adhesive rubber asphalt waterproof membrane by roller coating. Under the action, the film stock solution dries quickly to form a film on the surface of the coil.
[0030] Table 1 Formation conditions and properties of tear-free film
[0031] Coil temperature / ℃ Blowing air volume / m 3 / s Film thickness / μm lye pH Alkaline temperature / ℃ Dissolving time / h 95 2.5 20 9...
Embodiment 2
[0033] First, 100 parts of cardanol, 90 parts of formaldehyde aqueous solution (37%) and 2980 parts of polyvinyl alcohol aqueous solution (5%) are added to the reactor, and when the temperature rises to 60°C, an appropriate amount of alkaline solution (5% ) to maintain pH=8.5-9.0, react for 90min. Then add the remaining 100 parts of formaldehyde aqueous solution (37%), and continue to react at 80±2°C for 40 minutes to obtain the membrane stock solution.
[0034] Then neutralize the film stock solution to pH=7.0 first, then dilute to 5%, and apply it on the surface of the freshly formed self-adhesive rubber asphalt waterproof membrane by roller coating. Under the action, the film stock solution dries quickly to form a film on the surface of the coil.
[0035] Table 2 Formation conditions and properties of tear-free film
[0036] Coil temperature / ℃ Blowing air volume / m 3 / s Film thickness / μm lye pH Alkaline temperature / ℃ Dissolving time / h 85 3.0 30 9.0...
Embodiment 3
[0038] First, 100 parts of cardanol, 85 parts of formaldehyde aqueous solution (37%) and 3420 parts of polyvinyl alcohol aqueous solution (5%) are added to the reactor, and when the temperature is raised to 60°C, an appropriate amount of alkaline solution (5% ), to keep the pH=8.5-9.0, react for 80min. Then add the remaining 105 parts of formaldehyde aqueous solution (37%), and continue to react at 85±2°C for 70 minutes to obtain the membrane stock solution.
[0039] Then neutralize the film stock solution to pH = 7.0 first, then dilute to 5%, and apply it on the surface of the newly formed self-adhesive rubber asphalt waterproof membrane by roller coating. Under the action, the film stock solution dries quickly to form a film on the surface of the coil.
[0040] Table 3 Formation conditions and properties of tear-free film
[0041] Coil temperature / ℃ Blowing air volume / (m 3 / s) Film thickness / μm lye pH Alkaline temperature / ℃ Dissolving time / h 95 1.5...
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