A thermosetting resin composition with good insulation, prepreg and metal clad board
A thermosetting, composition technology, applied in metal layered products, layered products, chemical instruments and methods, etc., can solve problems such as poor insulation, and achieve the effects of improving workability, low friction coefficient, and good insulation
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Embodiment 1
[0046] The preparation of embodiment 1 filler A1-A4
[0047] Fillers A1-A4 were prepared by using the preparation method provided by the present invention with different raw material ratios according to the component contents of the fillers of the present invention, and their compositions and mass percentages are shown in Table 1.
Embodiment 2
[0063] The preparation of embodiment 2 resin composition
[0064] The fillers prepared in Example 1 and Comparative Example of the present invention were prepared into a resin glue solution for copper clad laminates with methyl ethyl ketone, in which the solid content accounted for 65%, and its components and contents are shown in Table 3.
[0065] table 3
[0066]
[0067]
[0068] The material used in the embodiment and its composition are as follows:
[0069] Thermosetting resin A is bisphenol A type epoxy resin produced by Dow Chemical, the trade name is DER530, and the epoxy equivalent is 435g / eq.
[0070] Thermosetting resin B is a novolac epoxy resin produced by Hexion Chemical Company of the United States (formerly Bolton Chemical Company of the United States and Beckett Company of Germany), the trade name is EPR627-MEK80, and its epoxy equivalent is between 160-250g / eq.
[0071]The curing agent is a phenolic resin curing agent produced by Hexion Chemical Compa...
Embodiment 3
[0073] Example 3 Copper-clad laminates were prepared using the fillers prepared in the present invention and the fillers prepared in the comparative example
[0074] (1) Glue making: Add the solvent into the batching container, and add the thermosetting resin, curing agent solution and curing accelerator solution respectively under stirring; after stirring for 2 hours, add the filler, continue stirring for 4-8 hours, take a sample to test the glue The gelling time (170°C constant temperature hot plate) is 200-300 seconds.
[0075] (2) Impregnation: Pass the reinforced material layer soaked in glue through a vertical or horizontal impregnation machine, and control the extrusion wheel speed, line speed, wind temperature and furnace temperature. The specific example of the vertical impregnation machine is : Extrusion wheel speed: -1.3~-2.5±0.1M / min; Main line speed: 4~18m / min; Air temperature: 120~170℃; Furnace temperature: 130~220℃, to make prepreg.
[0076] (3) Pressing: After...
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Abstract
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