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Mass spectrum analyzer and analyzing method thereof

A mass spectrometer and a series of technologies, which are applied in the field of mass analysis in analytical instruments, can solve the problems of low image current frequency, insufficient magnetic field strength in ion orbits, and low signal frequency, so as to improve the signal frequency of image current and prevent ion Effect of diffusion escape and uniform distribution of magnetic field intensity

Active Publication Date: 2013-11-27
常州磐诺仪器有限公司
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Problems solved by technology

[0008] The purpose of the present invention is to solve the problem that the superconducting magnet of the existing FTICR mass spectrometer is expensive, the magnetic field strength of the permanent magnet is insufficient, and the frequency of the image current is low
The invention provides a design scheme with compact structure and low cost, which solves the problem of insufficient magnetic field strength in the space where the ion orbit is located, and further uses multiple image current pickup electrodes to solve the problem of low signal frequency

Method used

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  • Mass spectrum analyzer and analyzing method thereof
  • Mass spectrum analyzer and analyzing method thereof

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Embodiment Construction

[0034]The present invention will be further described below in conjunction with the accompanying drawings, so that the structure and principle of this device and method can be clearly understood by those skilled in the art. It should be understood that the specific embodiments described here are only used to explain the present invention, not to limit the present invention.

[0035] The inventors found that if the ion orbital radius is excited by the cyclotron resonance method, it is necessary to provide a uniform high-intensity magnetic field distribution on the entire cross-section of the working chamber. However, in the image current acquisition stage after the ions are excited, the ions only move on the orbit with a larger radius, and the movement frequency has nothing to do with the magnetic field in the central region with a smaller radius. The present invention proposes a method for constructing a magnetic cyclotron mass spectrometer, which includes the use of a magneti...

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Abstract

The invention relates to the technical field of mass analysis of analytical instruments, in particular to a mass spectrum analyzer and an analyzing method thereof. The mass spectrum analyzer comprises a magnetic field generating device, a vacuum system, an ion source, an ion accelerator and a series of electrodes. The magnetic field generating device is used for forming a high-strength magnetic field in annular space, an annular axle line exists in the annular space, and magnetic lines of the high-strength magnetic field and the axle line are orthogonal; the vacuum system is used for forming ultrahigh vacuum in the annular space; the ion source is used for generating analyzed ions; the ion accelerator accelerates the analyzed ions which enter an ion annular motion track basically along the axle line and sustain circumnutation for a while; at least parts of the electrodes arranged around the annular axle line are used for detecting image charges induced on the ions in a circumnutation process. According to the mass spectrum analyzer and the analyzing method thereof, the image current signal frequency is improved effectively, the limit electrodes can prevent ions from being diffused and escaping, the magnetic field distribution is even, the mass spectrum quality is improved effectively, and the market prospect is good.

Description

[technical field] [0001] The invention relates to the technical field of mass analysis in analytical instruments, in particular to a mass spectrometer and an analysis method thereof. [Background technique] [0002] Mass spectrometer, also known as mass spectrometer, is an instrument used to separate and detect different chemical or biological components. It separates and detects substances according to the mass of atoms, molecules or molecular fragments of substances according to the state and results of the movement of charged particles in an electromagnetic field. composition. Magnetic mass spectrometer is a kind of mass spectrometer, which has experienced a long history of development. From the traditional magnetic deflection mass spectrometer and magnetic cyclotron mass spectrometer to the modern Fourier transform magnetic cyclotron resonance mass spectrometer (FTICR), they all use the movement of charged ions in a magnetic field to analyze their species. Mass resoluti...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01J49/38H01J49/00
Inventor 丁贤忠
Owner 常州磐诺仪器有限公司
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