Method for producing spherical furfuryl alcohol resin particles, spherical furfuryl alcohol resin particles produced thereby, spherical carbon particles and spherical activated carbon particles
一种糠醇树脂、制造方法的技术，应用在化学仪器和方法、碳的制备/纯化、碳化合物等方向
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1-
[0044] The dodecylbenzenesulfonic acid (pKa=-2) that drops into 0.15 mass parts in the reaction vessel that possesses thermometer, stirring device and reflux cooler is used as the acid catalyst (a) of resinization, further adds 80 mass parts water and After 100 parts by mass of furfuryl alcohol, stir and mix the contents by heating to 80°C and reacting for 1 hour, and then heating to 90°C and reacting (condensation resin) for 1 hour to obtain a furfuryl alcohol condensation product with a weight average molecular weight of 6700. resin. Next, 10 parts by mass of a 5% aqueous solution of gum arabic, 2.5 parts by mass of an aqueous solution of 10% dodecylbenzenesulfonic acid (pKa=-2) as an acid catalyst (b) for curing, and 8.25 parts by mass of water were added thereto. , stirring and mixing for granulation, and reacting at 95° C. for 3 hours (hardening reaction). After the reaction, the inside of the reaction container was cooled to room temperature, followed by filtration, was...
Embodiment 2-
[0047] After adding 0.2 parts by mass of oxalic acid (pKa=1.2), 80 parts by mass of water, and 100 parts by mass of furfuryl alcohol into a reaction vessel equipped with a thermometer, a stirring device and a reflux cooler, the mixed content was heated to 80° C. to react ( condensation resinization) for 2 hours to obtain a furfuryl alcohol condensation resin with a weight average molecular weight of 570. Next, 40 parts by mass of a 5% aqueous solution of gum arabic, 15 parts by mass of a 10% aqueous solution of p-toluenesulfonic acid (pKa=-2.8), and 18.5 parts by mass of water were added thereto to form a reaction system, which was granulated while stirring and mixing. It was reacted at 95° C. for 3 hours (curing reaction). After the above-mentioned reaction, the inside of the reaction container was cooled to room temperature, followed by filtration, washing, and drying, whereby the target furfuryl alcohol resin particles were produced. Then, confirm that the obtained resin p...
Embodiment 3-
[0050] After adding 0.2 parts by mass of oxalic acid (pKa=1.2), 80 parts by mass of water, and 100 parts by mass of furfuryl alcohol into a reaction vessel equipped with a thermometer, a stirring device and a reflux cooler, the mixed content was heated to 80° C. to react ( condensation resinization) for 2 hours to obtain a furfuryl alcohol condensation resin with a weight average molecular weight of 570. Next, 1 part by mass of a 5% aqueous solution of gum arabic, 2.5 parts by mass of a 10% aqueous solution of dodecylbenzenesulfonic acid (pKa=-2), and 16.8 parts by mass of water were added thereto, and stirred and mixed for granulation at 95 The reaction was carried out at °C for 3 hours (curing reaction). After the above-mentioned reaction, the inside of the reaction container was cooled to room temperature, followed by filtration, washing, and drying to produce the target furfuryl alcohol resin particles. Then, confirm that the obtained resin particles are spherical by SEM ...
PUM
| Property | Measurement | Unit |
|---|---|---|
| particle diameter | aaaaa | aaaaa |
| particle diameter | aaaaa | aaaaa |
| Weight-average Molecular Weight | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More