Ultraviolet light cured elastic polyurethane acrylate flat lacquer and preparation method thereof
A polyurethane acrylate, ultraviolet light technology, applied in the direction of polyurea/polyurethane coatings, coatings, etc., can solve problems such as low efficiency and pollution
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Embodiment 1
[0046] The present embodiment to the third embodiment are UV-curable polyurethane acrylate elastic hand-feel matt paints prepared by using different PCDL as soft segments and HEMA-terminated synthetic polyurethane acrylate as the matrix resin.
[0047] Polycarbonate diol T5651 (molecular weight 1000) is used as the soft segment, IPDI is the hard segment to synthesize semi-terminated polyurethane, 26 parts of polyurethane acrylate synthesized with HEMA end-capped, mixed reactive diluent (EOEOEA 20 parts, HDDA 10 parts, TPGDA 10 parts, TMP (3EO) TA 50 parts, PET4A 10 parts) 8 parts, elastic handle filler (black) 10 parts, TS-1004 parts, photoinitiator Irgacure 1842 parts, initially dispersed with a high-speed mixer at a speed of 2000-2500r / min , Add 50 parts of butyl acetate in batches, after all the addition is finished, stir at 3500-4000r / min for 30min to obtain slurry. Films are formed on PC boards and ABS boards by a knife coating method, baked at 50°C for 20 minutes, and then ...
Embodiment 2
[0049] Polycarbonate diol T5652 (molecular weight 2000) is used as the soft segment, IPDI is the hard segment to synthesize semi-terminated polyurethane, 26 parts of polyurethane acrylate synthesized with HEMA end-capped, mixed reactive diluent (EOEOEA 20 parts, HDDA 10 parts, TPGDA 10 parts, TMP (3EO) TA 50 parts, PET4A 10 parts) 8 parts, elastic handle filler (black) 10 parts, TS-1004 parts, photoinitiator Irgacure 1842 parts, initially dispersed with a high-speed mixer at a speed of 2000-2500r / min , Add 50 parts of butyl acetate in batches, after all the addition is finished, stir at 3500-4000r / min for 30min to obtain slurry. Films are formed on PC boards and ABS boards by a knife coating method, baked at 50°C for 20 minutes, and then cured under ultraviolet light to obtain an elastic touch paint film.
Embodiment 3
[0051] Polycarbonate diol G3452 (molecular weight 2000) is used as the soft segment, IPDI is the hard segment to synthesize semi-terminated polyurethane, 26 parts of polyurethane acrylate is synthesized with HEMA end-capped, mixed reactive diluent (EOEOEA 20 parts, HDDA 10 parts, TPGDA 10 parts, TMP (3EO) TA 50 parts, PET4A 10 parts) 8 parts, elastic handle filler (black) 10 parts, TS-1004 parts, photoinitiator Irgacure 1842 parts, initially dispersed with a high-speed mixer at a speed of 2000-2500r / min , Add 50 parts of butyl acetate in batches. After all the additions are completed, stir at 3500-4000r / min for 30min to obtain slurry. Films are formed on PC boards and ABS boards by a knife coating method, baked at 50°C for 20 minutes, and then cured under ultraviolet light to obtain an elastic touch paint film.
[0052] The physical and chemical indexes of the UV-curable polyurethane acrylate elastic touch matte paint obtained in the above examples are shown in Table 1:
[0053] T...
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