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Low-salt and low-alkali dyeing process of cellulose fiber fabrics with medium-temperature reactive dyes

A technology for cellulose fibers and reactive dyes, which is applied in the field of low-salt and low-alkali dyeing technology, can solve the problems of the limited effect of the amount of salt used for reactive dyes in ultrasonic dyeing machines, the inability to achieve industrial application, and the difficulty of functioning alone, and achieves heavy dyeing. Good presentability and dyeing fastness, beneficial to leveling and penetration dyeing, and the effect of reducing the amount of salt used for dyeing promotion

Active Publication Date: 2016-01-13
佛山市马大生纺织有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0014] However, practice has proved that the investment in low-salt and low-alkali dyeing equipment is large and the production efficiency is low, and the actual effect of reducing the amount of alkali used for dyeing is not clear
At the same time, the effect of ultrasonic dyeing machine on reducing the amount of salt used in reactive dyes is very limited, it is difficult to play a role alone, and industrial application cannot be realized in the short term

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0048] The raw materials for this dyeing process include:

[0049] 1. Fabric to be dyed: pure cotton bleached cloth 1000g

[0050] 2. Medium temperature reactive dye: Huntsman NOVACRONDEEPNIGHTS-R20g

[0051] 3. Neutral electrolyte: 360g of anhydrous sodium sulfate (ie 40g / L)

[0052] 4. Inorganic base: sodium carbonate 81g (ie 9g / L)

[0053] 5. Fiber modifier: Diethylenetriamine 40g

[0054] 6. Dye modifier: triethylamine 1g

[0055] 7. Softened water: the total hardness is 25ppmCaCO 3 Soft water 9000g

[0056] The specific steps of the dyeing process:

[0057] (1) Pretreatment of the fabric to be dyed: modifying the cellulose fiber fabric to be dyed with a fiber modifier to obtain a partially aminated modified cellulose fiber fabric to be dyed, specifically:

[0058] (1.1) Put 8800g of demineralized water, diethylenetriamine, and pure cotton bleached cloth into the dyeing machine;

[0059] (1.2) Raise the temperature to 45°C, keep warm and maintain the circulation of...

Embodiment 2

[0073] The raw materials for this dyeing method include:

[0074] 1. Fabric to be dyed: pure cotton bleached mercerized cloth 1000g

[0075] 2. Medium temperature reactive dye: ArgazolBlueBP30g

[0076] 3. Neutral electrolyte: 530g of anhydrous sodium sulfate (53g / L)

[0077] 4. Inorganic base: sodium carbonate 110g (ie 11g / L)

[0078] 5. Fiber modifier: Triethylenetetraaminopropyldimethoxysilane 30g

[0079] 6. Dye modifier: trimethylamine 2g

[0080] 7. Softened water: the total hardness is 20ppmCaCO 3 Soft water 10000g

[0081] The specific steps of the staining technique:

[0082] (1) The step of pretreating the fabric to be dyed: modifying the cellulose fiber fabric to be dyed with a fiber modifier to obtain a partially aminated modified cellulose fiber fabric to be dyed, specifically:

[0083] (1.1) Put 9700g of demineralized water, triethylenetetraaminopropyl dimethoxysilane, and pure cotton bleached mercerized cloth into the dyeing machine;

[0084] (1.2) Heat ...

Embodiment 3

[0096] Embodiment 3 The low-salt and low-alkali dyeing technology of medium-temperature reactive dyestuff of the present invention to cellulose fiber fabric

[0097] The raw materials for this dyeing method include:

[0098] 1. Fabric to be dyed: polyester (content 20%) cotton (content 80%) bleached mercerized cloth 1000g

[0099] 2. Medium temperature reactive dye: Huntsman NOVACRONDEEPNIGHTS-R40g

[0100] 3. Neutral electrolyte: 520g of anhydrous sodium sulfate (ie 65g / L)

[0101] 4. Inorganic base: sodium carbonate 100g (ie 12.5g / L)

[0102] 5. Fiber modifier: Triethylenetetraaminopropyltriethoxysilane 25g

[0103] 6. Dye modifier: N-methyldiethanolamine 3.3g

[0104] 7. Softened water: the total hardness is 25ppmCaCO 3 Soft water 8000g

[0105] The specific steps of the staining technique:

[0106] (1) The step of pretreating the fabric to be dyed. In this step, the fabric to be dyed is modified with a fiber modifier to obtain a partially aminated modified cellulose...

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PUM

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Abstract

The invention relates to a low-salt and low-alkali dyeing process with a mesothermal type active dye of a cellulosic fiber fabric. The low-salt and low-alkali dyeing process comprises the following steps: modifying a cellulosic fiber fabric to be dyed by a fiber modifying agent to prepare a partially-aminated modified cellulosic fiber fabric to be dyed; modifying the mesothermal type active dye by a dye modifying agent to prepare an activated and modified mesothermal type active dye; and carrying out low-salt and low-alkali dyeing on the cellulosic fiber fabric, namely carrying out the low-salt and low-alkali dyeing on the partially-aminated modified cellulosic fiber fabric to be dyed by the activated and modified mesothermal type active dye in the presence of neutral electrolyte, inorganic alkalis and water. According to the dyeing technology, the use amount of the neutral electrolyte and the inorganic alkalis can be reduced and the dyeing temperature can be reduced by about 10 DEG C; the dyed cellulosic fiber fabric has high coloring depth, good dyeing fastness and excellent dyeing reproducibility; the low-salt and low-alkali dyeing process can be used for dyeing various cellulosic fiber fabrics by the mesothermal type active dye.

Description

technical field [0001] The invention relates to a low-salt and low-alkali dyeing process for reactive dyes on cellulose fibers or blended fabrics mainly composed of cellulose fibers, in particular to a low-salt and low-alkali dyeing process for medium-temperature reactive dyes on cellulose fiber fabrics. Background technique [0002] In the current production practice, reactive dyes are the most commonly used dyes for dyeing cellulose fiber textiles, and the most used ones are medium-temperature reactive dyes. A lot of alkali and salt are used in the dyeing process of medium-temperature reactive dyes. In order to solve the environmental pollution and cost pressure problems caused by the traditional high-salt and high-alkali dyeing process of reactive dyes, the low-salt and low-alkali dyeing technology of reactive dyes is always relevant. research and development focus in the field. At present, the low-salt and low-alkali dyeing process of reactive dyes is mainly divided int...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06P1/38D06P3/66D06P5/22D06P1/673D06M13/332D06M13/513D06M101/06D06M101/32
Inventor 权衡韩静李新平章靖黎谦姜会钰朱慧慧倪丽杰吴丹雷开臣
Owner 佛山市马大生纺织有限公司
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