Nanostructured article and method of making the same
A kind of product, sub-micron technology, applied in the direction of nanotechnology, nano optics, nanotechnology, etc., can solve the problems of high haze, lower display quality, etc., and achieve the effect of enhancing optical performance and low streak effect
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[0270] Process 1: Vacuum plasma treatment plasma heating batch reactor
[0271] A batch plasma system (available from Oerlikon, St. Petersburg, FL under the trade designation "PLASMATHERM" (model 3032)) configured for reactive ion etching (RIE) with 68.6 cm (27 in.) low-level power electrodes and central air pump. The chamber was pumped by a dry mechanical pump (available as model iQDP80 from Edwards Vacuum) via a Roots blower (available as model EH1200 from Edwards Vacuum, Tewsbury, MA). Do the pumping. RF power was provided by a 3 kW, 13.56 Mhz solid-state generator (commercially available under the trade designation "RFPP" (model RF30H) from Advanced Energy, Fort Collins, CO) through an impedance-matched network. The system has a nominal base pressure of 5 mTorr. The flow rate of the gas was controlled by a flow rate controller (commercially available from MKS Instruments, Woburn, MA) under the trade designation "MKS 1179".
[0272] A substrate for plasma treatment is...
example 18
[0303] 450 g of 1-methoxy-2-propanol, 6 g of 3-(methacryloxy)propyltrimethoxysilane, and 0.16 g of a 5% aqueous solution of hindered amine nitroxide inhibitor (“PROSTAB5128”) Mix together with 190nm silica dispersion ("MP2040") while stirring. The solution was sealed in a jar and heated to 80°C and held at that temperature for 16 hours. Water and 1-methoxy-2-propanol were removed from the mixture by rotary evaporation. The resulting dry, surface-functionalized silica particles were redispersed into an 88 / 12 1-methoxy-2-propanol / water mixture, then sonicated and filtered to form a 42.4% by weight solid dispersion.
[0304] A monomer blend of pentaerythritol triacrylate, 1,6-hexanediol diacrylate and isobornyl acrylate ("SR444", "SR238", "SR506", respectively) was mixed in a 40 / 40 / 20 ratio with Dispersions of 190 nm silica particles modified with 3-(methacryloxy)propyltrimethoxysilane were blended to form 65% by weight of 3-(methacryloxy)propyltrimethoxysilane Oxysilane-modif...
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