Cuprous oxide nanowire material and preparation method thereof
A technology of cuprous oxide and nanowires, which is applied in the field of nanomaterials and chemical materials, and can solve problems such as long time
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Embodiment 1
[0019] Add 500 ml of sodium hydroxide aqueous solution (concentration: 0.01 mol / liter) to the reaction bottle, then add 0.001 mol of cuprous thiocyanate powder (0.123 g), apply ultrasonic waves for 1 hour, filter, wash, and dry to obtain the oxidized Cuprous nanowire material. The crude yield is greater than 80%.
[0020] figure 1 It is the result of XRD analysis, which proves that the main component of the product is cuprous oxide, but also contains a small amount of unreacted cuprous thiocyanate in the product.
[0021] figure 2 is a typical SEM image of cuprous oxide nanowire material, showing random packing of cuprous oxide nanowires. The width of cuprous oxide nanowires is less than 50 nanometers, and the length can reach several micrometers or even longer.
[0022] image 3 The SEM image of the cuprous oxide nanowire material at a higher resolution shows that the width of the nanowire is less than 50 nanometers, and the length has exceeded the imaging range.
Embodiment 2
[0024] Add 500 ml of sodium hydroxide aqueous solution (concentration: 0.02 mol / liter) to the reaction bottle, then add 0.001 mol of cuprous thiocyanate powder (0.123 g), apply ultrasonic waves for 1 hour, filter, wash, and dry to obtain the oxidized Cuprous nanowire material. The crude yield is greater than 75%.
[0025] Figure 4 It is the result of XRD analysis, which proves that the product is cuprous oxide.
[0026] The SEM image of the cuprous oxide nanowire material is similar to Example 1.
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