Yellowing process of viscose production

A viscose fiber and process technology, which is applied in the yellowing process field of viscose fiber production, to achieve the effects of shortening the dissolution cycle, stable quality, and not easy to trip

Active Publication Date: 2014-08-27
CHENGDU GRACE FIBER +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005]1. The production cycle of the yellowing machine is long and the production capacity is low;
[0006]2. When the yellowing machine is discharging, the current of the discharge pump and the pulverizer is high, the energy consumption is high, and it is easy to trip, resulting in the extension of the yellowing cycle;
[0007]3. The viscose ball and dissolved alkaline water are mixed unevenly, which may easily cause the discharge pump to be stuck and the equipment to run unstable
This patent adopts the combination of dry and wet method yellowing, the phenomenon of viscose clumping is obvious, and the diameter of clumping can reach more than 1 meter, which is not conducive to the subsequent dissolution and grinding process

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] A yellowing process for viscose fiber production, the process steps are as follows:

[0031] A After the yellowing reaction is over, add the primary dissolved alkali and the secondary dissolved alkali to the yellowing machine successively, and add the primary dissolved water while adding the secondary dissolved alkali;

[0032] B Open the discharge valve, the cellulose sulfonate in the yellowing machine flows from the discharge pipeline to the pulverizer, while opening the discharge valve, add secondary dissolved water to the discharge pipeline;

[0033] C When the output reaches more than 90%, add flushing alkali to the yellowing machine, and the end of a yellowing cycle is the end of the output.

Embodiment 2

[0035] The implementation mode of this embodiment is basically the same as embodiment 1, on this basis:

[0036] The mass ratio of the primary dissolved base to the secondary dissolved base is 1:3.

Embodiment 3

[0038] The implementation mode of this embodiment is basically the same as embodiment 1, on this basis:

[0039] The mass ratio of the primary dissolved base to the secondary dissolved base is 1:1.

[0040] After the primary dissolving alkali is added, the speed of the yellowing machine is increased to a high speed, and then the secondary dissolving alkali is added into the yellowing machine.

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Abstract

The invention provides a yellowing process of viscose production. The process comprises the following steps: (A) after yellowing reaction is ended, adding primary dissolution alkali and secondary dissolution alkali into a yellowing machine successively, and adding primary dissolution water while adding secondary dissolution alkali; (B) opening a discharging valve to enable cellulose sulfonate in the yellowing machine to flow to a grinding machine from a discharging pipeline, and adding secondary dissolution water into the discharging pipeline while opening the discharging valve; (C) when the discharging rate is more than 90%, adding flushing alkali into the yellowing machine, and fully discharging, namely ending a yellowing cycle. According to the process, the dissolution water is added while the dissolution alkali is added, so that the time for separately adding the dissolution water is saved and the purposes of shortening the production cycle of the yellowing machine, increasing the production capacity of the yellowing machine, improving the operating stability of equipment and reducing the current consumption of the equipment and the energy consumption are achieved.

Description

Technical field [0001] The invention is the field of adhesive fiber production, which involves a yellowing technology for the production of adhesive fiber. Invention background [0002] As the saying goes: "Seven -point glue, three -point spinning." It can be seen that the quality of adhesive glue has a great impact on the quality of fiber products, and the decisive effect on the quality of sticky glue is the control of the yellow chemical process.The length of the cycle of the yellowing, the control of temperature during the yellowization process is a key issue that determines the quality of adhesion. [0003] The steps of the existing technologies' sticky fiber yellow chemical technology are: After the yellowing reaction is over, the dissolved alkali, secondary dissolved alkali, and dissolved water are added from the top of the yellow chemical machine toThe adhesive glue production in the short fiber of the glue, and then open the ingredients of the material pump. When it is o...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08B9/02
Inventor 江洪陈涛
Owner CHENGDU GRACE FIBER
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