Adhesive composition and adhesive film for semiconductor and semiconductor device
An adhesive film, semiconductor technology, applied in the direction of film/sheet adhesive, non-polymer adhesive additives, adhesive types, etc., can solve the problems of inability to remove voids and inability to ensure fluidity Achieving good equipment identification, increased efficiency and productivity
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Examples
Embodiment 1 to 2
[0146] Examples 1 to 2: Preparation of Adhesive Compositions for Semiconductors
[0147] As listed in Table 1, add solvent (cyclohexanone) to thermoplastic resin, epoxy resin, phenol curing agent, amine curing agent, curing accelerator, filler and silane coupling agent so that the solid content in the solution is 20wt% , and then sufficiently kneaded these components with a bead mill, thereby preparing an adhesive composition for semiconductors.
Embodiment 1
[0164] Each adhesive composition prepared in Examples 1 and 2 and Comparative Examples 1, 2 and 3 was deposited onto a PET release film with a coater, and then dried in an oven at 100° C. for 10 to 30 minutes to provide Adhesive film with 5 μm thick adhesive layer. Furthermore, an adhesive film having an adhesive layer having a thickness of 10 μm and having the same components as in Example 1 was prepared in Example 3.
experiment example
[0165] Experimental Example: Evaluation of Physical Properties of Adhesive Compositions and Adhesive Films Prepared in Examples and Comparative Examples
[0166] The physical properties of each adhesive composition in Examples 1 to 3 and Comparative Examples 1, 2, and 3 or an adhesive film prepared using the same were evaluated by the following methods, and the results are shown in Table 2.
[0167] Table 2
[0168] project
condition
unit
Example 1
Example 2
Example 3
Comparative example 1
Comparative example 2
Comparative example 3
chip shear strength
260℃
Kgf / chip
2.5
2.4
2.8
3.0
0.6
2.5
%
28
25
33
24
25
11
Storage modulus after 1 cycle (A)
175℃
10 6 Dyne / cm 2
3.2
2.7
3.2
4.4
1.6
2.8
Storage modulus after 4 cycles (B)
175℃
10 6 Dyne / cm 2
4.4
4.3
4.4
8.2
3.2
4.5
...
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