Method for preparing alumina rock mineral polymer organic-inorganic composite material by impregnation method
A technology of inorganic composite materials and mineral polymers, which is applied in the field of preparation of aluminum rock mineral polymer organic-inorganic composite materials by impregnation method, which can solve the problems of insufficient mechanical properties such as strength and insufficient wide application range, and achieve simple preparation process , high economic value and environmental benefits, the effect of rich resources
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Embodiment 1
[0019] Take 40×40×160mm sample of aluminous rock polymer material for drying treatment, prepare an MMA (methyl methacrylate) organic solution containing 0.3% benzoyl peroxide curing agent, and immerse the dried sample after drying and cooling. After immersion in MMA (methyl methacrylate) organic solution at room temperature and pressure for 4 days, it was taken out, prepolymerized at 80 °C for 2 hours, then quickly cooled to room temperature, then polymerized at 50 °C for 24 hours, and then kept at 80 °C After 2h, the reaction was completed, that is, the organic-inorganic composite material was obtained.
[0020] Its compressive strength reaches 116.1MPa, its flexural strength reaches 31.5MPa, and the material has excellent mechanical properties.
Embodiment 2
[0022] Take 40 × 40 × 160 mm aluminum rock polymer material samples for drying treatment, prepare epoxy resin organic solution containing 0.3% benzoyl peroxide curing agent, and immerse the dried samples in epoxy resin organic solution after drying and cooling. The solution was soaked at room temperature and pressure for 5 days, taken out, prepolymerized at 100 °C for 2 hours, then quickly cooled to room temperature, then polymerized at 65 °C for 24 hours, and then kept at 50 °C to 100 °C for 2 hours to complete the reaction, that is, Organic-inorganic composite materials were prepared.
[0023] Its compressive strength reaches 114.9MPa, its flexural strength reaches 31.4MPa, and the material has excellent mechanical properties.
Embodiment 3
[0025] A 40×40×160mm sample of aluminum rock polymer material was taken and dried, and an epoxy resin organic solution containing 0.3% benzoyl peroxide curing agent was prepared. After drying and cooling, the dried sample was immersed in the amino resin organic solution. After immersion at normal temperature and pressure for 6 days, take it out, prepolymerize at 120 °C for 2 hours, then quickly cool to room temperature, then polymerize at 80 °C for 24 hours, and then keep it at 120 °C for 2 hours to make the reaction complete, that is, the organic- Inorganic composite materials.
[0026] Its compressive strength reaches 115.4MPa, its flexural strength reaches 31.2MPa, and the material has excellent mechanical properties.
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