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A transparent heating furnace

A heating furnace and transparent technology, which is applied in the field of heating furnaces, can solve the problems of long distance between the inner tube and the outer tube, increased cost, and it is not conducive to adjusting the angle of the observation window, etc., and achieves the effect of thermal insulation.

Active Publication Date: 2016-04-06
INST OF PROCESS ENG CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the furnace body of this patent is composed of three quartz tubes, inner, middle and outer, as well as a furnace cover and a furnace bottom, and has a complex structure.
On the one hand, the diameter of the furnace body is large, and the distance between the inner tube and the outer tube is far away, which is not conducive to close-range visual observation
On the other hand, the furnace bottom and the furnace cover are connected as a whole through the support rod, and the outer tube cannot be rotated, which is not conducive to adjusting the angle of the observation window and affects the practicability of the product
Moreover, thermocouples, heating furnace wires and power cord connectors are located inside the furnace cover, resulting in consumables such as thermocouples, heating furnace wires and internal components that cannot be replaced, thereby affecting the service life of the transparent heating furnace
In addition, when used with the magnetic field coil, due to the large diameter of the outer tube, in order to ensure the normal use of the magnetic field coil, a magnetic field coil with a larger inner diameter is required, resulting in a sudden increase in the weight and volume of the magnetic field coil and an increase in cost

Method used

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  • A transparent heating furnace
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0063] The diameter of the inner tube is 66mm and the height is 300mm; the diameter of the outer tube is 110mm and the height is 300mm. A support frame is provided on the outer wall of the inner tube, and there is a card slot on the support frame. The heating element is a silicon carbide rod with a diameter of 8mm. The thermal insulation coating on the outer wall of the outer tube is a gold-plated coating with a thickness of 20nm; A metal-free observation window (length 60mm, width 10mm) is provided along the radial direction. The inner tube has a thickness of 8 mm and the outer tube has a thickness of 3 mm. The temperature control meter uses Xiamen Yudian program temperature control device.

[0064] The implementation results are as follows:

[0065] The heating power can reach 2200W, the maximum heating temperature is 1000°C, it takes 40 minutes to program the temperature from room temperature to 1000°C, and the error is less than 1°C; it can run stably for a long time at ...

Embodiment 2

[0067] The diameter of the inner tube is 180mm and the height is 1000mm; the diameter of the outer tube is 200mm and the height is 1000mm. The outer wall of the inner tube is provided with a spiral groove, and the heating element is Cr20Ni80 electric furnace wire with a diameter of 2.0mm. The thermal insulation coating on the outer wall of the outer tube is a nickel-tungsten alloy coating with a thickness of 50nm; There is a metal-free observation window (length 500mm, width 30mm). The inner tube has a thickness of 20 mm and the outer tube has a thickness of 10 mm. The temperature control meter uses Xiamen Yudian program temperature control device.

[0068] The implementation results are as follows:

[0069] The heating power can reach 10000W, the maximum heating temperature is 1000°C, it takes 20 minutes to program the temperature from room temperature to 1000°C, and the error is less than 1°C; it can run stably for a long time at 950°C, and the heating current is not highe...

Embodiment 3

[0071] The inner tube diameter is 30mm and the height is 200mm; the outer tube diameter is 50mm and the height is 200mm. The outer wall of the inner tube is provided with a spiral groove, and the heating element is a silicon-molybdenum rod with a diameter of 3mm. The thermal insulation coating on the outer wall of the outer tube is a zirconia coating with a thickness of 10nm; Observation window with or without metal coating (length 30mm, width 10mm). The inner tube has a thickness of 6 mm and the outer tube has a thickness of 3 mm. The temperature control meter uses Xiamen Yudian program temperature control device.

[0072] The implementation results are as follows:

[0073] The heating power can reach 1000W, the maximum heating temperature is 950°C, it takes 45 minutes to program the temperature from room temperature to 900°C, and the error is less than 1°C; it can run stably for a long time at 900°C, and the heating current is not higher than 3A. Under any heating condition...

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PUM

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Abstract

The invention relates to a transparent heating furnace, in particular to a transparent heating furnace for a fluidized bed reactor. A furnace body is provided with an inner pipe and an outer pipe sequentially from inside to outside; a heating element is arranged on the outer wall of the inner pipe; a thermal insulation coating is arranged on the outer wall of the outer pipe; an observation window is formed in the longitudinal middle part of the thermal insulation coating; the inner pipe and the outer pipe are fixed through an inner ring groove and an outer ring groove in a furnace lid and a furnace bottom respectively; the outer pipe can rotate along the outer ring groove; the heating power of the transparent heating furnace for the fluidized bed is 500-5,000W, the heating temperature is not lower than 900DEG C, and the temperature rate is adjustable. The transparent heating furnace is simple in structure and small in size, components are easy to assemble and replace, the transparent heating furnace can serve as a heating device for scientific research in a laboratory and is particularly used in the field of fluidization research for observing particle flow and fluidization actions under the heating condition.

Description

technical field [0001] The invention relates to a heating furnace for scientific research and industrial use in the fields of chemistry, chemical industry, energy, metallurgy, pharmacy and nano material preparation, and more specifically relates to a transparent heating furnace used in the field of fluidization. Background technique [0002] Particle fluidization technology has the advantages of high mass transfer and heat transfer rate and uniform gas-solid reaction temperature, which makes the fluidized bed reactor based on particle fluidization widely used in coal chemical industry, petrochemical industry, iron and steel metallurgy, biomedicine, and nanomaterials. Traditional and emerging industries such as preparation have a wide range of applications. But in the gas-solid bubbling fluidized bed, the gas will form bubbles, and the particles will form agglomerates due to the inelastic collision between particles, the adhesion of particles during the reaction process, the ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): F27B15/00F27B15/02F27B15/14
Inventor 李军朱庆山李洪钟芦亚军
Owner INST OF PROCESS ENG CHINESE ACAD OF SCI
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