Synthesis method of heavy metal chelating agent
A technology of heavy metal chelating agent and synthesis method, applied in chemical instruments and methods, water pollutants, water/sewage treatment, etc., can solve problems such as wastewater pollution, achieve the effect of solving pollution problems and improving flocculation and sedimentation performance
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Embodiment 1
[0018] A kind of synthetic method of heavy metal chelating agent provided by the present embodiment comprises the following steps:
[0019] The first step is to add excess carbon disulfide to polyvinylamine with active amino groups under the environment of pH 9, so that polyvinylamine reacts with sufficient carbon disulfide to obtain an intermediate product, wherein the average molecular weight of polyvinylamine 250,000;
[0020] In the second step, sodium hydroxide powder is added to the intermediate product and stirred, and then solid-liquid separation is carried out to obtain a heavy metal chelating agent.
Embodiment 2
[0022] A kind of synthetic method of heavy metal chelating agent provided by the present embodiment comprises the following steps:
[0023] In the first step, under an environment with a pH value of 8, an excessive amount of carbon disulfide is added to the polyallylamine having an active amino group, so that the polyallylamine reacts with a sufficient amount of carbon disulfide to obtain an intermediate product, wherein the average molecular weight of the polyallylamine is 220,000;
[0024] In the second step, potassium hydroxide powder is added to the intermediate product and stirred, and then solid-liquid separation is carried out to obtain the heavy metal chelating agent.
Embodiment 3
[0026] A kind of synthetic method of heavy metal chelating agent provided by the present embodiment comprises the following steps:
[0027] In the first step, under an environment with a pH value of 10, excessive carbon disulfide is added to polyvinylamine having an active amino group, so that polyvinylamine reacts with a sufficient amount of carbon disulfide to obtain an intermediate product, wherein the average molecular weight of polyvinylamine 280,000;
[0028] In the second step, ferric hydroxide powder is added to the intermediate product and stirred, and then solid-liquid separation is carried out to obtain the heavy metal chelating agent.
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