Polyurethane-coated slow-release fertilizer and preparation method thereof
A coated slow-release, polyurethane technology, applied in the direction of layered/coated fertilizers, fertilization devices, fertilizer mixtures, etc., can solve the problems of poor elasticity, poor degradability, and easy to be dissolved by water of inorganic coated fertilizers. Good low temperature resistance, simple and reasonable process, good degradability
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[0031] Example 1
[0032] The parts by weight of each raw material are:
[0033] Polyether polyol (functionality is preferably 3, molecular weight is preferably 1500) 100 parts, diisocyanate (TDI-80) 45 parts, epoxy resin (E-44) 22 parts, curing agent (E-100) 42 parts.
[0034] The preparation method of polyurethane coated slow-release fertilizer is:
[0035] (1) Preparation of epoxy modified prepolymer
[0036] Add the measured polyether polyol into the flask, reduce pressure to -0.090MPa, stir and heat to 110℃, vacuum dehydration for 2.4h, then cool to 40℃, add epoxy resin, stir for 30min, add diisocyanate, temperature control React at 85°C for 2.5 hours; after the reaction is completed, start to cool down and vacuum degas for 20 minutes, cool to room temperature and discharge, to obtain an epoxy modified prepolymer with a -NCO of 7%;
[0037] (2) Preparation of polyurethane coated fertilizer
[0038] A modified fluidized bed parallel spray method is used for coating. When coating, an...
Example Embodiment
[0040] Example 2
[0041] The parts by weight of each raw material are:
[0042] 95 parts of polyether polyol (DDL-1000D), 40 parts of diisocyanate (TDI-80), 20 parts of epoxy resin (E-44), and 40 parts of curing agent (E-100).
[0043] The preparation method of polyurethane coated slow-release fertilizer is:
[0044] (1) Preparation of epoxy modified prepolymer
[0045] Add the measured polyether polyol into the flask, reduce pressure to -0.085MPa, stir and heat to 100℃, vacuum dehydration for 3h, then cool to 45℃, add epoxy resin, stir for 20min, add diisocyanate, and control the temperature at 80°C, react for 3h; after the reaction is complete, start to cool down and vacuum degas for 30min, cool down to room temperature and discharge, to obtain epoxy modified prepolymer with -NCO of 5%;
[0046] (2) Preparation of polyurethane coated fertilizer
[0047] A modified fluidized bed parallel spray method is used for coating. When coating, an independent spray system sprays the prepolymer ...
Example Embodiment
[0049] Example 3
[0050] The parts by weight of each raw material are:
[0051] 100 parts of polyether polyol (DDL-1000D), 50 parts of diisocyanate (TDI-80), 25 parts of epoxy resin (E-44), and 45 parts of curing agent (E-100).
[0052] The preparation method of polyurethane coated slow-release fertilizer is:
[0053] (1) Preparation of epoxy modified prepolymer
[0054] Add the measured polyether polyol into the flask, reduce pressure to -0.098MPa, stir and heat to 120°C, vacuum dehydration for 2h, then cool to 50°C, add epoxy resin, stir for 25min, add diisocyanate, and control the temperature at 90°C, react for 2h; after the reaction is completed, start cooling and vacuum degassing for 10 minutes, cooling to room temperature and discharging to obtain an epoxy modified prepolymer with a -NCO of 9%;
[0055] (2) Preparation of polyurethane coated fertilizer
[0056] A modified fluidized bed parallel spray method is used for coating. When coating, an independent spray system sprays the...
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