Method for simultaneously detecting phenol, NNK and benzo-[a]-pyrene in main stream smoke of cigar by using gas chromatography-tandem mass spectrum
A technology of cigarette mainstream smoke and tandem mass spectrometry, which is applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve the problems of complicated and time-consuming processing, and achieve the effects of simple sample pretreatment, improved analysis throughput, and good repeatability
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[0019] The present invention will be further described below in conjunction with embodiment:
[0020] Equilibrate and extract the samples of the cigarettes to be tested, use a rotary smoking machine to smoke according to the standard conditions specified in YC / T29-1996, and use Cambridge filters to capture the particulate matter in the mainstream smoke of 20 cigarettes.
[0021] Put the Cambridge filter with the particulate phase trapped into a 250 mL ground-mouth Erlenmeyer flask, add 40 mL of methanol, add deuterated phenol (1 mg / mL), deuterated NNK (1 μg / mL), Deuterated benzo[a]pyrene (1 μg / mL) methanol solution 200 μL; ultrasonically extract the Erlenmeyer flask at room temperature for 30 min, take 2 mL of the extract, pass through a 0.22 μm organic phase filter membrane, and use a chromatographic vial Samples were collected for GC-MS / MS analysis.
[0022] GC-MS / MS analysis conditions: chromatographic inlet temperature: 260 ℃; injection volume: 1 μL; injection method: spl...
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