Nanometer wire purifying device and purifying method

A purification device and nanowire technology, applied in nanotechnology, nanotechnology, nanotechnology for materials and surface science, etc., can solve the problems of separation, difficult nanowires and nanoparticle integrity, and achieve simple process and low cost , the effect of high yield

Active Publication Date: 2015-05-06
青岛康普顿石油化工有限公司
View PDF4 Cites 12 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The purification method of nanowires reported in the literature is mainly to use the different sedimentation velocity of nanowires and n

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Nanometer wire purifying device and purifying method
  • Nanometer wire purifying device and purifying method
  • Nanometer wire purifying device and purifying method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] Such as figure 1 As shown, a nanowire purification device: including a first container 1, a second container 2, a third container 3, a delivery pump 4 and a tubular filter 5, and the tubular filter 5 is on the side near the outlet of the main pipe A side wall outlet is opened on the wall, wherein the first container 1 is connected to the delivery pump 4, and the delivery pump 4 is connected to the inlet of the tubular filter 5, and the side wall outlet of the tubular filter 5 is connected to the second container 2, The main pipe outlet of the tube filter 5 is connected to the third container 3; the delivery pump 4 is a peristaltic pump; the first container 1, the second container 2, and the third container 3 are all beakers.

[0021] Purification method: add 300ml of absolute ethanol to 500ml of the first container 1, then add 5g of silver nanowires (length greater than 10 microns) and nanoparticles (particle diameter less than 500 nanometers) mixture under stirring, an...

Embodiment 2

[0023] The purification device is the same as in Example 1.

[0024] Purification method: Add 300ml of distilled water to 500ml of the first container 1, then add 5g of copper nanowire (length greater than 5 microns) and nanoparticle (particle size less than 300nm) mixture under stirring, mix uniformly to form a suspension, and then send it to the pump 4 Insert a tubular filter 5 with a pore size of 3 microns, adjust the pressure difference between the inlet of the tubular filter 5 and the outlet of the main pipe, so that part of the liquid flows out along the side wall outlet of the tubular filter 5, and the remaining liquid is filtered by the tubular filter. The outlet of the main pipe of the device 5 flows out, and the second container 2 and the third container 3 respectively collect the liquid flowing out from the outlet of the side wall of the tubular filter 5 and the outlet of the main pipe; the liquid collected by the third container 3 is filtered to obtain a brown-red s...

Embodiment 3

[0026] The purification device is the same as in Example 1.

[0027] Purification method: Add 300ml cyclohexane into 500mL first container 1, then add 5g of nickel sulfide nanowire (length greater than 500nm) and nanoparticle (particle size less than 50nm) mixture under stirring, after mixing uniformly to form a suspension A tubular filter with a pore size of 50 nanometers is injected by the delivery pump 4, and the pressure difference between the inlet of the tubular filter 5 and the outlet of the main pipe is adjusted, so that part of the liquid flows out along the side wall outlet of the tubular filter 5, and the remaining liquid is obtained by The outlet of the main pipe of the tubular filter 5 flows out, and the second container 2 and the third container 3 respectively collect the liquid flowing out from the outlet of the side wall of the tubular filter 5 and the outlet of the main pipe; the liquid collected by the third container 3 is filtered to obtain a black solid powd...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
Lengthaaaaaaaaaa
Particle sizeaaaaaaaaaa
Lengthaaaaaaaaaa
Login to view more

Abstract

The invention belongs to the technical field of novel functional nanometer material preparation method and discloses a nanometer wire purifying device and a purifying method. The invention comprises the following steps: adding a liquid medium into a first container; adding a nanometer wire to be purified under stirring, wherein the nanometer wire to be purified is a mixture of nanometer wires and nanometer particles; uniformly mixing to form a suspending liquid and injecting the suspending liquid into a tubular filter by a transfer pump; adjusting pressure differences between inlet and outlet ends of the tubular filter to make part of the liquid to leak from a side wall of the tubular filter and rest of the liquid to leak from the outlet of the tubular filter; collecting the liquid leaking from the side wall and the outlet of the tubular filter by a second container and a third container respectively; and filtering the liquid collected in the third container to obtain solids to obtain the purified nanometer wire. According to the invention, mesh diameter of the tubular filter is bigger than particle diameters of the nanometer particles but smaller than length of the nanometer wire. The purifying device and the purifying method of the invention are characterized by simple device, simple process, low cost, high product yield and the like. The purifying device and the purifying method of the invention can be used to obtain nanometer wires of high purity.

Description

technical field [0001] The invention belongs to the technical field of preparation of novel functional nanometer materials, and in particular relates to a nanowire purification device and a purification method. Background technique [0002] As a one-dimensional nanomaterial, nanowires have completely different properties from zero-dimensional nanoparticles, and have a wide range of applications in solar cells, electronic materials, conductive materials, catalytic materials, polymer composite materials, and other fields. In recent years, the preparation methods of nanowires have attracted great attention of researchers. The preparation methods reported at present are mainly divided into template method and seed method. The template method is limited by the template and the template needs to be removed after the preparation is completed. Suitable for large-scale industrial preparation. The principle of preparing nanowires by the seed method is that the nanowires grow epitaxia...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): C01G53/11B22F1/00B82Y30/00
Inventor 张玉娟张晟卯张治军张平余
Owner 青岛康普顿石油化工有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap