pdmo/tio 2 Nanowire Anode Catalyst for Direct Methanol Fuel Cells
A methanol fuel cell and nanowire technology, applied to battery electrodes, circuits, electrical components, etc., to reduce costs and improve the ability to resist CO poisoning
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Embodiment 1
[0020] (1) TiO 2 Preparation of nanowires: using sol-gel method and hydrothermal synthesis method. Dissolve the calculated amount of butyl titanate in a certain amount of absolute ethanol, add dropwise a mixture of absolute ethanol, glacial acetic acid and deionized water under stirring, and continue stirring after hydrolysis to form a sol, and let it stand for 2- After 3 days, the powder obtained after vacuum drying at 80 °C for 8-10 hours is ground and then calcined in air at 400-600 °C for 3 hours in a muffle furnace to obtain TiO 2 Nano powder. The consumption molar ratio of butyl titanate, dehydrated alcohol, glacial acetic acid, deionized water when preparing sol is: n 钛酸丁酯 :n 无水乙醇 :n 冰醋酸 :n 去离子水 =1:20~40:1~2.5:2~6. TiO will be produced 2 Add the nano powder into the autoclave, add 10 mol / L NaOH solution, stir, heat to 180-220°C, react for 48 hours, centrifuge, wash with dilute hydrochloric acid and deionized water for 6-8 times until the filtrate is Neutral, aft...
Embodiment 2
[0030] In step (5), according to the last synthesized catalyst W PdMo =3%, molar ratio n Pd :n Mo =1:1, all the other are with embodiment 1.
Embodiment 3
[0032] In step (5), according to the last synthesized catalyst W PdMo =5%, molar ratio n Pd :n Mo =3:7, all the other are with embodiment 1.
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