Telbivudine orally-disintegrating tablet and preparation method thereof
A technology of orally disintegrating tablets and telbivudine, applied in the field of medicine
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Embodiment 1
[0029] The weight ratios of the raw materials are: Telbivudine 100, lactose 48, sorbitol 130, microcrystalline cellulose 110, low-substituted hydroxypropyl cellulose 26, saccharin sodium 1.0, and magnesium stearate 5.
[0030] Preparation:
[0031] (1) Telbivudine, microcrystalline cellulose, low-substituted hydroxypropyl cellulose, sorbitol, and magnesium stearate are dried at 110°C for 1 hour, crushed through a 100 mesh sieve, and lactose and saccharin sodium are crushed through a 100 mesh sieve spare;
[0032] (2) Weigh telbivudine, sorbitol, lactose, sodium saccharin, 1 / 4 amount of low-substituted hydroxypropyl cellulose, 1 / 4 amount of microcrystalline cellulose and mix in proportion to obtain a mixture;
[0033] (3) Add 50% ethanol solution to the mixture material obtained in step (2) to make suitable soft materials, granulate with a 32-mesh sieve, dry the wet granules at 40 ±5°C, and size them with a 32-mesh sieve;
[0034] (4) Mix the particles obtained in step (3) with the bala...
Embodiment 2
[0037] The weight ratios of the raw and auxiliary materials are: Telbivudine 100, lactose 60, sorbitol 150, microcrystalline cellulose 118, low-substituted hydroxypropyl cellulose 28, saccharin sodium 0.9, magnesium stearate 5.6.
[0038] Preparation:
[0039] (1) Telbivudine, microcrystalline cellulose, low-substituted hydroxypropyl cellulose, sorbitol, and magnesium stearate are dried at 110°C for 1 hour, crushed through a 100 mesh sieve, and lactose and saccharin sodium are crushed through a 100 mesh sieve spare;
[0040] (2) Weigh telbivudine, sorbitol, lactose, sodium saccharin, 1 / 4 amount of low-substituted hydroxypropyl cellulose, 1 / 4 amount of microcrystalline cellulose and mix in proportion to obtain a mixture;
[0041] (3) Add 50% ethanol solution to the mixture material obtained in step (2) to make suitable soft materials, granulate with a 32-mesh sieve, dry the wet granules at 40 ±5°C, and size them with a 32-mesh sieve;
[0042] (4) Mix the particles obtained in step (3) w...
Embodiment 3
[0045] The weight ratio of the raw and auxiliary materials is: Telbivudine 100, lactose 50, sorbitol 125, microcrystalline cellulose 109, low-substituted hydroxypropyl cellulose 25, saccharin sodium 1.4, magnesium stearate 4.8.
[0046] Preparation:
[0047] (1) Telbivudine, microcrystalline cellulose, low-substituted hydroxypropyl cellulose, sorbitol, and magnesium stearate are dried at 110°C for 1 hour, crushed through a 100 mesh sieve, and lactose and saccharin sodium are crushed through a 100 mesh sieve spare;
[0048] (2) Weigh telbivudine, sorbitol, lactose, sodium saccharin, 1 / 4 amount of low-substituted hydroxypropyl cellulose, 1 / 4 amount of microcrystalline cellulose and mix in proportion to obtain a mixture;
[0049] (3) Add 50% ethanol solution to the mixture material obtained in step (2) to make suitable soft materials, granulate with a 32-mesh sieve, dry the wet granules at 40 ±5°C, and size them with a 32-mesh sieve;
[0050] (4) Mix the particles obtained in step (3) wit...
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