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Method for extracting light-color soapnut saponin

A technology of sapindus sapindis and an extraction method, which is applied in the field of extraction of light-colored sapindus saponins, can solve the problems of dark color of saponins, deepened color of products, darkened colors, and the like, and achieves the effects of light color and low cost.

Active Publication Date: 2015-05-27
QUANGANG PETROCHEM RES INST OF FUJIAN NORMAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although these methods have obtained Sapindus saponins, because they are in a heated state for a long time in the extraction process, the color of saponins is dark, which seriously affects the color matching effect of the use process, so it is widely used to prepare light-colored sapinsia saponins. The premise of application, there are two main reasons for the darkening of Sapindus saponin. One is because the phenolic hydroxyl and carboxyl groups in its own structure are oxidized to carbonyl or quinone groups under long-term heating conditions, which makes the color darker. The second is that when extracting sapindus saponins, some water-soluble impurities such as sugars are also dissolved, and coking occurs under long-term heating conditions, resulting in deepening of product color

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] Pulverize 100g of dried Sapindus japonica peel to 20 mesh, add 1000ml of water, stir at 80°C, and at the same time pass in nascent (that is, just prepared) hydrogen, and keep the speed of hydrogen at 100ml / min, After extraction for 2 hours, solid-liquid separation was performed, the pH of the extract was adjusted to 6.0, and 10 g of 35% hydrogen peroxide was added for oxidative decolorization for 0.5 hours; then the supernatant was spray-dried to obtain saponin powder.

Embodiment 2

[0015] Pulverize 100 g of dried Sapindus japonica peel to 40 mesh, add 800 ml of water, stir at 70 ° C, and at the same time pass in nascent (that is, just prepared) hydrogen, and keep the speed of passing hydrogen at 70 ml / min, After extraction for 5 hours, solid-liquid separation was performed, the pH of the extract was adjusted to 7.0, and 8 g of 45% hydrogen peroxide was added for oxidative decolorization for 1 hour; then the supernatant was spray-dried to obtain saponin powder.

Embodiment 3

[0017] Pulverize 100 g of dried Sapindus japonica peel to 50 mesh, add 600 ml of water, stir at 60 ° C, and at the same time pass in the hydrogen of the initial ecology (that is, just prepared), keep the speed of passing hydrogen at 40 ml / min, After 8 hours of extraction, solid-liquid separation was performed, the pH of the extract was adjusted to 8.0, and 6 g of 55% hydrogen peroxide was added for oxidative decolorization for 1.5 hours; then the supernatant was spray-dried to obtain saponin powder.

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Abstract

The invention relates to a method for extracting light-color soapnut saponin. The method comprises the following main process steps: crushing 100 - parts of dried soapberry peel by weight into powder with the granularity of 20-80 meshes, adding 100-1000 parts of water, and uniformly stirring at the temperature of 40-80 DEG C; introducing nascent-state hydrogen gas which is newly prepared, maintaining the hydrogen introducing speed to be 2-100ml / min, extracting the solution after 2-15 hours, performing solid-liquid separation, regulating the pH value of the extracting solution to 6.0-10.0, adding 2-10 parts of 35-70 percent hydrogen peroxide for oxidative decoloration for 0.5-2.0 hours; and performing spray drying on the supernatant, thereby obtaining the saponin powder. The prepared soapnut saponin is light in color, low in cost, high-efficiency and environment-friendly.

Description

technical field [0001] The invention provides a method for extracting sapindus saponin, which belongs to the technical field of biochemical product research. Background technique [0002] Sapindus muKorossi Gaerth (Sapindus muKorossi Gaerth), also known as soap tree or hand-washing fruit, is a deciduous tree belonging to Sapindus family Sapindus. It is distributed in Southeast Asian countries, Taiwan Province of my country and the provinces south of the Huaihe River. Sapindus aril is rich in glycosides, mainly triterpene saponins and sesquiterpene glycosides, which have good foaming and decontamination properties, and can be used as natural active substances in shampoos and various It also has physiological effects such as antibacterial and antipruritic, and can be used in the field of biomedicine. The extraction methods of Sapindus Sapindus total saponins mainly include organic solvent extraction and water extraction. The organic solvent extraction method uses organic solv...

Claims

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Application Information

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IPC IPC(8): C07G99/00C07J63/00C07H15/256C07H1/08
Inventor 陈登龙王珊珊刘金玲王勇黄秀萍
Owner QUANGANG PETROCHEM RES INST OF FUJIAN NORMAL UNIV
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