Method for degumming fragrant rap oil through enzymic process

A technology of rapeseed oil and strong aroma, which is applied in the direction of fat oil/fat refining and fat production, which can solve the problems of low refining yield, coking of equipment, and affecting the effect of degumming, and achieve low oil content on dry basis and high oil foot volume The effect of reducing and avoiding oil loss

Inactive Publication Date: 2015-05-27
国粮武汉科学研究设计院有限公司
View PDF5 Cites 10 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Whether it is hydration degumming or acid degumming, it cannot remove the non-hydratable phospholipids well, which affects the effect of degumming
If the degumming effect is not good, it will increase the burden of subsequent decolorization, deacidification and deodorization, and increase the loss of oil refining and the consumption of auxiliary materials
Difficulty in filtration, coking of equipment, increased consumption of white clay, low refining yield, and high phosphorus content is often accompanied by more metal ions, resulting in easy rancidity and color reversion of oil, affecting oil quality and economic benefits
At the same time, it is easy to have adverse effects on the equipment, such as coking of equipment affects the heat transfer effect, the filter screen is easily blocked and affects the filtration speed, resulting in difficult decolorization and increased clay consumption.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method for degumming fragrant rap oil through enzymic process

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] 1. Put the crude rapeseed oil obtained by cleaning and frying the seeds and pressing the oil making process to stand for 24 hours, then centrifuge or mechanically filter out most of the impurities contained in it, and the impurity-removed crude oil passes through the heat exchanger in the enzymatic hydrolysis tank Heat to 40°C-45°C.

[0023] 2. Dissolving the citric acid solid in demineralized water to prepare a citric acid solution with a mass concentration of 50% in the acid tank for subsequent use.

[0024] 3. Add 50% citric acid solution according to the proportion of 0.4% of the oil weight, and stir and mix. The stirring and mixing speed is 50r / min, and the time is 60 minutes.

[0025] 4. Transfer the oil and acid mixture in the acid reaction tank to the enzyme reaction tank, add soft water, the temperature of the soft water is 5°C higher than the oil temperature, the amount of soft water added is about 1.8% of the oil, stir well and evenly, and then press 0.13% o...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention discloses a method for degumming fragrant rap oil through an enzymic process. The method is characterized by comprising the following steps: heating the squeezed fragrant crude rap oil without impurities to about 40 DEG C, adding a 50% citric acid aqueous solution according to 0.1% by weight of the oil, mixing the 50% citric acid aqueous solution with the fragrant crude rap oil, mixing and stirring at a rate of 50-60r/min, and stirring for one hour; adding soft water according to 1.8% by weight of the oil, adding a phospholipase A, phospholipase B or phospholipase C solution diluted to 100 times according to 0.13% of the total mass of oil and water, simultaneously stirring and reacting for 60 minutes at a rate of 40-50r/min under the temperature of 30-50 DEG C, filtering or centrifugally separating, and drying to obtain the finished product of the fragrant rap oil.

Description

technical field [0001] The invention relates to a method for degumming fragrant rapeseed oil, in particular to a method using phospholipase A 1 or phospholipase A 2 A method for removing phospholipid colloids in fragrant rapeseed oil. Background technique [0002] The existing method for preparing fragrant rapeseed oil by degumming crude fragrant rapeseed oil as raw material is to adopt hydration degumming and acid degumming. Water degumming is to use the hydrophilicity of phospholipids and other colloids, add hot water to the oil under stirring, so that the phospholipids absorb water and swell and condense, and the expanded oil can absorb other colloids in the oil, so that the colloids in the oil Solubility decreased, separated from oil by natural sedimentation. Acid degumming is to heat the crude oil first, then fully mix it with phosphoric acid or citric acid solution to react, then add water and then separate. [0003] Hydration degumming can only remove hydratable p...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C11B3/00C11B3/04
CPCC11B3/001C11B3/003C11B3/04
Inventor 龚任周俊梅李维琳
Owner 国粮武汉科学研究设计院有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products