Preparation method of hemp carbon polyester fiber with high-efficient adsorption and hygroscopic properties

A technology of hygroscopicity and polyester fiber, which is applied in the field of hemp charcoal/polyester fiber preparation, can solve problems such as insufficient adsorption capacity, and achieve the effect of high-efficiency adsorption and hygroscopicity

Active Publication Date: 2015-07-01
江苏微笑新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The present invention aims at the shortcomings of insufficient moisture absorption and adsorption capacity of fibers, adopts hemp charcoal with a large specific surface area as an additive material, uses nano-silica powder for modification, and then blends and granulates with polyester chips, and finally the obtained The polyester fiber of the hemp charcoal is subjected to alkali washing treatment to remove the silica powder as a modification component, re-exposing the pore structure of the hemp charcoal powder, and at the same time increasing the pore structure of the fiber, endowing the fiber with stronger adsorption and moisture absorption ability

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] 1) Put nano-scale hemp charcoal powder with a particle size of 300nm, γ-aminopropyltriethoxysilane and nano-scale silicon oxide powder with a particle size of 50nm in water according to the mass ratio of 1:0.05:0.2, and set the temperature at room temperature Stirring, the stirring time is 10min, and the stirring speed is 50rpm, so that the nano-scale silicon oxide powder is attached to the surface pores of the nano-scale hemp charcoal powder, and then the unattached nano-scale silicon oxide powder is filtered by a filter paper with a pore size of 300nm. In addition to filtering and drying to obtain a composite powder;

[0023] 2) Dry the composite powder and polyester chips obtained in step 1) at 100°C for 2 hours, then transfer to a vacuum drying oven for 12 hours at 140°C, and then put the composite powder and polyester chips in Preliminary mixing at 180°C and 50rpm stirring speed, and finally inject the obtained mixed powder into a twin-screw extruder to extrude and...

Embodiment 2

[0027] 1) Put nano-sized hemp charcoal powder with a particle size of 700nm, γ-glycidyl etheroxypropyl trimethoxysilane and nano-sized silicon oxide powder with a particle size of 300nm in water according to the mass ratio of 1:0.4:0.2 , stirring at room temperature, the stirring time is 60min, and the stirring speed is 200rpm, so that the nano-scale silicon oxide powder is attached to the surface pores of the nano-scale hemp charcoal powder, and then the unattached nano-scale silicon oxide powder is removed by a filter cloth with a pore size of 300nm. The powder is filtered and dried to obtain a composite powder;

[0028] 2) Dry the composite powder and polyester chips obtained in step 1) at 150°C for 6 hours, then transfer to a vacuum drying oven for 24 hours at 170°C, and then put the composite powder and polyester chips in Preliminary mixing at 240°C and a stirring speed of 200rpm, and finally inject the resulting mixed powder into a twin-screw extruder to extrude and gran...

Embodiment 3

[0032] 1) The nanoscale hemp charcoal powder with a particle size of 400nm, γ-(methacryloyloxy)propyltrimethoxysilane and the nanoscale silicon oxide powder with a particle size of 100nm according to the mass ratio of 1:0.4: 1 Put it into water, stir at room temperature, the stirring time is 20min, and the stirring speed is 80rpm, so that the nano-scale silicon oxide powder is attached to the surface pores of the nano-scale hemp charcoal powder, and then use filter paper or filter cloth with a pore size of 300nm to remove the non-adhered The nano-scale silicon oxide powder is filtered and dried to obtain a composite powder;

[0033] 2) Dry the composite powder and polyester chips obtained in step 1) at 120°C for 3 hours, then transfer to a vacuum drying oven for 20 hours at 150°C, and then put the composite powder and polyester chips in Preliminary mixing at 200°C and 60rpm stirring speed, and finally inject the obtained mixed powder into a twin-screw extruder to extrude and gra...

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Abstract

The invention discloses a preparation method of a hemp carbon polyester fiber with high-efficient adsorption and hygroscopic properties. The preparation method comprises the following steps: (1) feeding nanoscale hemp carbon powder, a silane coupling agent and nanoscale silica powder to water, stirring at room temperature, adhering the nanoscale silica powder to holes in the surface of the nanoscale hemp carbon powder, filtering and drying to obtain composite powder; (2) extruding and granulating the obtained composite powder and polyester slices to obtain functional master batches; (3) melting and spinning the obtained functional master batches and the polyester slices to obtain the polyester fiber containing the composite powder; and (4) carrying out alkali washing, removing the nanoscale silica powder adhered to hemp carbon, and forming a hole structure in the polyester fiber, which extends to the surface of the polyester fiber, washing and drying to obtain the hemp carbon/polyester fiber with the hole structure. The hemp carbon/polyester fiber prepared by the invention has high-efficient adsorption and hygroscopic properties, and can be widely applied to the fields such as clothes and home textiles.

Description

technical field [0001] The invention belongs to the technical field of functional fiber production, and relates to a preparation method of hemp charcoal / polyester fiber with high-efficiency adsorption and moisture absorption properties. Background technique [0002] Polyester and polyester fiber have flourished since the 1970s and have been widely used in clothing and industrial fields. Polyester fiber has good comprehensive properties, and its strength, wear resistance, resilience and dimensional stability can better meet the needs of various purposes. But polyester fiber is a typical hydrophobic fiber, its moisture regain is only about 0.4%, and polyester fiber generally has a smooth surface and no hole structure. It is poor in wearing comfort when used as a wearing material, and it is easy to produce stuffy feeling when wearing it in a humid and hot state. Affect mood. At the same time, in the field of textile and clothing, it is no longer satisfied with traditional non...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F6/92D01F1/10
Inventor 谈辉郑耀伟王彪张瑞民
Owner 江苏微笑新材料科技有限公司
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