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Equipment and method used for solid particle or solid-liquid mixture washing and purification

A technology of solid-liquid mixture and solid particles, which is applied in the direction of liquid cleaning methods, separation methods, chemical instruments and methods, etc., can solve the problems of low material concentration, high cost, and limited washing effect, and achieve simple equipment structure and easy operation. The effect of easy control and short production process

Inactive Publication Date: 2015-08-05
CHANGSHA DESIGN & RES INST OF CHEM IND MIN +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The traditional equipment for solid-liquid mixture washing generally adopts the pump plus centrifuge system, but the amount of washing liquid (or washing water) in the centrifuge is small, the washing and purification effect is limited, and it is difficult to meet the high purity requirements of the product
Traditional equipment for solid washing generally uses a washing tank plus a pump and a centrifuge. However, if the amount of washing liquid added to the washing tank is too large, the concentration of the material will be too low, which will affect the normal operation of the centrifuge. On the contrary, if the amount of washing liquid added is small, the washing effect will be poor.
The above-mentioned solid and solid-liquid mixture washing and purification equipment has a long process, high cost and limited washing effect

Method used

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  • Equipment and method used for solid particle or solid-liquid mixture washing and purification

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Experimental program
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Effect test

Embodiment 1

[0025] Embodiment 1: the equipment embodiment that is used for solid particle or solid-liquid mixture washing purification

[0026] Such as figure 1 As shown, the embodiment of the equipment for washing and purifying solid particles or solid-liquid mixtures of the present invention includes: a tank body 1, a spray device 2, an electro-hydraulic push rod 3 and a limit switch 4; the spray device 2 is located in the tank Above the body 1; the inside of the tank body 1 is provided with a filter layer 11, a filtrate chamber 12 is provided under the filter layer 11, and a drain port 13 is provided at the bottom of the filtrate chamber 12; a rotating shaft 14 is provided at the bottom of the tank body 1, and the tank body 1 The bottom is connected with the electro-hydraulic push rod 3; the limit switch 4 is set on the tank body 1; the electro-hydraulic push rod 3 can drive the tank body 1 to turn around the rotating shaft 14, and the turning angle is from the central axis of the ta...

Embodiment 2

[0027] Embodiment 2: Embodiment 1 equipment is used for the method embodiment I of solid particle washing purification

[0028] (1) Spray washing: the potassium chloride solid particle material (purity 90wt%) placed on the filter layer 11 in the tank body 1 with an average particle diameter of 0.3 mm is statically sprayed and washed twice by the spray device 2, The first washing liquid is the washing mother liquid, and the second washing liquid is clear water, which is used as the washing mother liquid of the next batch of materials after washing, and left on the filter layer 11 after spraying and washing, and the filter layer 11 has a pore size less than 0.3 mm; (2) Water control and draining: the solid particle material after step (1) spraying and washing was left to stand for 0.3h, and then water control and draining was performed. Enter the filtrate chamber 12, and discharge from the discharge port 13 below the filtrate chamber 12; (3) Turn over and unload: start the ele...

Embodiment 3

[0029] Embodiment 3: Embodiment 1 equipment is used for the method embodiment II of solid-liquid mixture washing purification

[0030] (1) Filtration: transport the solid-liquid mixture material containing 30wt% potassium nitrate (the average diameter of potassium nitrate solid particles is 0.2mm) into the tank body 1, and let it stand on the filter layer 11 for 0.05h, and the seeped liquid is filtered The layer 11 enters the filtrate chamber 12, and is discharged from the drain port 13 below the filtrate chamber 12, and the filter cake is left on the filter layer 11; (2) Spray washing: the filter cake obtained in step (1) is statically sprayed by the spray device 2 Drenching and washing 3 times, the first two washing liquids are the washing mother liquor, the third washing liquid is clear water, and the clear water is used as the washing mother liquor of the next batch of materials after washing, and is left on the filter layer 11 after spraying and washing. The pore size o...

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Abstract

The invention discloses equipment and a method used for solid particle or solid-liquid mixture washing and purification. The equipment comprises a tank body, a spray device, an overturning device and a limit switch; the spray device is arranged above the tank body; a filter layer is arranged in the tank body, a filtrate chamber is arranged below the filter layer, and a liquid drain hole is formed in the bottom of the filtrate chamber; a rotating shaft is arranged at the bottom of the tank body, and the bottom of the tank body is connected with the overturning device; the limit switch is arranged on the tank body or overturning device. The method includes that (1) filtering, to be specific, placing solid-liquid mixture on the filter layer, wherein the liquid enters the filtrate chamber through the filter layer and is drained through the liquid drain hole; (2) spray washing, to be specific, carrying out spray washing on solid granular material or the filter cake of the step (1); (3) water controlling and draining, to be specific, carrying out water controlling and draining on the washed solid granular material or filter cake; (4) overturning to discharge material, to be specific, starting the overturning device to discharge the solid granular material or filter cake from the tank. The equipment cost is low; the method is short in flow, high in automatic degree and high in washed product purity.

Description

technical field [0001] The invention relates to a purification equipment and method, in particular to a purification equipment and method for solid particles or solid-liquid mixture. Background technique [0002] In actual production, there are many products that need to improve their purity, such as most inorganic salts and a small amount of organic products. The traditional equipment for washing solid-liquid mixture generally adopts the pump plus centrifuge system, but the amount of washing liquid (or washing water) in the centrifuge is small, the washing and purification effect is limited, and it is difficult to meet the high purity requirements of the product. Traditional equipment for solid washing generally uses a washing tank plus a pump and a centrifuge. However, if the amount of washing liquid added to the washing tank is too large, the concentration of the material will be too low, which will affect the normal operation of the centrifuge. On the contrary, if the am...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D29/01B01D29/78B01D29/94B08B3/02
Inventor 杨灿辉杨晓烽郭立戴斌联邓定军茆晓宝荣大林顾健
Owner CHANGSHA DESIGN & RES INST OF CHEM IND MIN
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