Polyimide film with low dielectric constant, and manufacturing method therefor
A polyimide film, polyimide technology, applied in chemical instruments and methods, electronic equipment, other household appliances, etc., can solve problems such as high dielectric constant and high dissipation coefficient
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Embodiment 1
[0053] Preparation of the first polyimide slurry: put 15.661 kg of TFMB and 132.6 kg of DMAc into a 200L reactor. After stirring at 30°C until completely dissolved, 21.63 kg of 6FDA was added. The monomer accounted for 22wt% of the total weight of the reaction solution. Then, add 15.98 kilograms of PTFE powder (accounting for 30wt% of the total monomer weight), keep stirring, and continue to react at 25°C for 24 hours to obtain the slurry of the first polyimide, which can be obtained at 25°C The rotational viscosity is 200,000cps.
[0054] Preparation of the second polyimide slurry: repeat the preparation steps of the first polyimide layer in Example 1, but without adding PTFE.
[0055] Preparation of polyimide film: The above-mentioned polyimide slurry is configured in the form of "second slurry-first slurry-second slurry", and is coated in a three-layer co-extrusion method, in continuous The polyimide film was prepared in the formula preparation process. The total thickn...
Embodiment 2
[0057] The first polyimide slurry: the monomer composition was changed to 19.492 kg of TFMB and 17.819 kg of BPDA. The monomer accounted for 22wt% of the total weight of the reaction solution.
[0058] The slurry of the second polyimide: with embodiment 1.
[0059] All the other ingredients and steps are the same as in Example 1.
Embodiment 3
[0061] The first polyimide slurry: the monomer components were changed to 11.61 kg of ODA and 25.66 kg of 6FDA. The monomer accounted for 22wt% of the total weight of the reaction solution.
[0062] The slurry of the second polyimide: with embodiment 1.
[0063] All the other ingredients and steps are the same as in Example 1.
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