A kind of fabric smoothing agent and preparation method thereof
A technology for a smoothing agent and fabric, applied in the field of a smoothing agent for fabrics and its preparation, can solve the problems of high use environment requirements, poor stability of the smoothing agent, easy falling off, etc., and achieves easy industrial production, safe and environmentally friendly raw materials, and simple preparation method. Effect
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Embodiment 1
[0023] (1) Weigh 60kg of simethicone oil, 5kg of dimethylformamide, 3kg of silicon dioxide with a diameter of 18 nanometers and 0.5kg of triethylenetetramine, mix well, add bis-(phenyldimethylsiloxane ) methylsilanol 8kg, three (trifluoropropyl) trimethylcyclotrisiloxane 3kg, mix 8 minutes in high-speed shearing machine;
[0024] (2) Slowly add the mixture of 2-heptadecyl imidazole 1.2kg, sodium pyrophosphate 0.5kg and adipic acid dihydrazide 0.02kg under the stirring condition of 1800 rpm in a high-speed mixer at 55°C, The temperature was kept at 50° C. for 3 hours to obtain a smoothing agent for fabrics.
[0025] The performance test results of the smoothing agent for fabrics are shown in Table 1.
Embodiment 2
[0027] (1) Weigh 60kg of simethicone oil, 8kg of dimethylformamide, 3kg of silicon dioxide with a diameter of 18 nanometers and 0.5kg of triethylenetetramine, mix well, add bis-(phenyldimethylsiloxane ) methylsilanol 11kg, three (trifluoropropyl) trimethylcyclotrisiloxane 3kg, mixed in a high-speed shear for 8 minutes;
[0028] (2) Slowly add the mixture of 2-heptadecyl imidazole 1.2kg, sodium pyrophosphate 0.5kg and adipic acid dihydrazide 0.02kg under the stirring condition of 1800 rpm in a high-speed mixer at 55°C, The temperature was kept at 50° C. for 3 hours to obtain a smoothing agent for fabrics.
[0029] The performance test results of the smoothing agent for fabrics are shown in Table 1.
Embodiment 3
[0031] (1) Weigh 45kg of simethicone oil, 5kg of dimethylformamide, 5kg of silicon dioxide with a diameter of 45 nanometers and 1.8kg of triethylenetetramine, mix well, add bis-(phenyldimethylsiloxane ) methylsilanol 8kg, three (trifluoropropyl) trimethylcyclotrisiloxane 3kg, mix 8 minutes in high-speed shearing machine;
[0032] (2) at 75 DEG C, slowly add the mixture of 2-heptadecyl imidazole 1.2kg, sodium pyrophosphate 0.5kg and adipic acid dihydrazide 0.8kg under the stirring condition of 2500 rpm in a high-speed mixer, The temperature was kept at 70° C. for 1.5 hours to obtain a smoothing agent for fabrics.
[0033] The performance test results of the smoothing agent for fabrics are shown in Table 1.
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