Ag-loaded C-doped TiO2 nano-particle visible-light-driven photocatalyst and use thereof
A nanoparticle and metal-loaded technology, which is applied in the field of C-doped TiO2 nanoparticle visible light catalyst, can solve the problem of low visible light activity, achieve the effect of improving photocatalytic activity, reducing the bandgap width, and facilitating separation
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Embodiment 1
[0021] A C-doped TiO loaded with metallic Ag 2 Nano particle visible light catalyst, its preparation method is as follows:
[0022] 1) Dissolve 1g of glucose in 40mL of isopropanol and stir. After the glucose is completely dissolved, slowly add 6mL of isopropyl titanate and continue to stir. After mixing evenly, add 6mL of glacial acetic acid, then stir vigorously for 10min, and seal the reaction device, stirred and aged at room temperature for 24h, and obtained carbon-doped TiO 2 Precursor sol;
[0023] 2) Doping the prepared carbon TiO 2 The precursor sol was dried at 60°C for 3h, then calcined in a muffle furnace at 400°C for 2h, and ground to obtain C-doped TiO with a particle size of 5-10nm 2 nanoparticles;
[0024] 3) Dissolve 0.0787g of silver nitrate in 100ml of water, add 1g of C-doped TiO obtained in step 2) 2 nanoparticles, first stirred for 30min to make the Ag + Adsorption on C-doped TiO 2 The surface of the nanoparticles, and then irradiated with ultraviol...
Embodiment 2
[0027] A C-doped TiO loaded with metallic Ag 2 Nano particle visible light catalyst, its preparation method is as follows:
[0028] 1) Dissolve 0.5g of glucose in 20mL of isopropanol and stir. After the glucose is completely dissolved, slowly add 5mL of isopropyl titanate and continue stirring. Reactor, stirred and aged at room temperature for 20h, prepared carbon-doped TiO 2 Precursor sol;
[0029] 2) Doping the prepared carbon TiO 2 The precursor sol was dried at 50°C for 5h, then calcined in a muffle furnace at 350°C for 3h, and ground to obtain C-doped TiO with a particle size of 5-20nm 2 nanoparticles;
[0030] 3) Dissolve 0.0315g of silver nitrate in 100ml of water, add 1g of C-doped TiO obtained in step 2) 2 nanoparticles, first stirred for 10min to make the Ag + Adsorption on C-doped TiO 2 The surface of the nanoparticles, and then irradiated with ultraviolet light with a wavelength of 250 nm, so that the Ag + Photoreduction to metal Ag, and finally filtered, w...
Embodiment 3
[0033] A C-doped TiO loaded with metallic Ag 2 Nano particle visible light catalyst, its preparation method is as follows:
[0034] 1) Dissolve 2g of glucose in 50mL of isopropanol and stir. After the glucose is completely dissolved, slowly add 10mL of isopropyl titanate and continue stirring. After mixing evenly, add 10mL of glacial acetic acid, then vigorously stir for 30min, and seal the reaction device, stirred and aged at room temperature for 30h to prepare carbon-doped TiO 2 Precursor sol;
[0035] 2) Doping the prepared carbon TiO 2 The precursor sol was dried at 80°C for 1h, then calcined in a muffle furnace at 500°C for 1h, and ground to obtain C-doped TiO with a particle size of 5-20nm 2 nanoparticles;
[0036] 3) Dissolve 0.0157g of silver nitrate in 100ml of water, add 1g of C-doped TiO obtained in step 2) 2 nanoparticles, first stirred for 30min to make the Ag + Adsorption on C-doped TiO 2 The surface of the nanoparticles, and then irradiated with ultraviol...
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