Preparation method of cellulose fabric having antibacterial and inflaming-retarding functions

A cellulose fabric and functional technology, applied in the field of preparation of cellulose fabrics, can solve the problems of easy adsorption of fabrics, affecting human health, breeding bacteria, etc.

Inactive Publication Date: 2015-09-16
ANHUI AGRICULTURAL UNIVERSITY +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Moreover, because the application of fabrics is closely related to people's daily life, and as a wearable product, it is common to be in contact with the skin. Therefore, people's requirements for the antibacterial performance of fabrics are getting higher and higher. Nowadays, fabrics have begun to appear on the market. Some fabrics with antibacterial function have been introduced, but because the fabric itself is easy to absorb and breed bacteria and fungal microorganisms, especially in underwear and medical fabrics, if the antibacterial effect is not good, it will greatly affect personal health, so it can be improved. The flammable properties of pre-cellulose fibers and the cellulose fabrics with antibacterial properties have become a research hotspot in this field.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Preparation method of cellulose fabric having antibacterial and inflaming-retarding functions
  • Preparation method of cellulose fabric having antibacterial and inflaming-retarding functions
  • Preparation method of cellulose fabric having antibacterial and inflaming-retarding functions

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Chitosan phosphate is according to following parts by weight:

[0030] Chitosan 15 parts

[0031] 20 parts of urea

[0032] Phosphoric acid 90 parts

[0033] Dimethylformamide 360 ​​parts

[0034] Mix and prepare, place at 95°C for 4 hours, filter, then wash with 50% (w / w) isopropanol aqueous solution for 3 times, and dry at 55°C;

[0035] Then dissolve chitosan phosphate with a concentration of 2% in a solution of 2% butane tetracarboxylic acid, add sodium hypophosphite with a concentration of 2% to the solution to prepare a fabric treatment solution, and then immerse the cotton fabric in the fabric treatment solution and take it out Afterwards, it was rolled dry, treated at 80°C for 3 minutes to remove water, and then treated at 150°C for 2 minutes to further remove water.

[0036] The cotton fabrics prepared above were subjected to limiting oxygen index measurement and antibacterial test respectively, compared with cotton fabrics treated with chitosan phosphate, ...

Embodiment 2

[0041] Chitosan phosphate is according to following parts by weight:

[0042] Chitosan 30 parts

[0043] 60 parts of urea

[0044] Phosphoric acid 60 parts

[0045] Dimethylformamide 300 parts

[0046] Prepare by mixing, place at 105°C for 6 hours, filter, then wash 4 times with 50% (w / w) isopropanol aqueous solution, and dry at 65°C;

[0047] Then dissolve chitosan phosphate with a concentration of 6% in a solution of 8% butane tetracarboxylic acid, add sodium hypophosphite with a concentration of 8% to the solution to prepare a fabric treatment solution, and then immerse the cotton fabric in the fabric treatment solution and take it out Afterwards, it was rolled dry, treated at 90°C for 5 minutes to remove water, and then treated at 170°C for 3 minutes to further remove water.

[0048] The above-mentioned cotton fabrics were carried out to measure the limiting oxygen index respectively, and carried out the antibacterial test, compared with the cotton fabrics without addi...

Embodiment 3

[0053] Chitosan phosphate is according to following parts by weight:

[0054] Chitosan 23 parts

[0055] 40 parts of urea

[0056] Phosphoric acid 75 parts

[0057] 332 parts of dimethylformamide

[0058] Mix and prepare, place at 100°C for 5 hours, filter, then wash with 50% (w / w) isopropanol aqueous solution for 4 times, and dry at 60°C;

[0059]Then dissolve chitosan phosphate with a concentration of 2% in a solution of 6% butane tetracarboxylic acid, add sodium hypophosphite with a concentration of 6% to the solution to prepare a fabric treatment solution, and then immerse the linen fabric in the fabric treatment solution and take it out Afterwards, it was dried by rolling, treated at 85°C for 3 minutes to remove water, and then treated at 160°C for 2 minutes to further remove water.

[0060] The flax fabrics prepared above were measured for limiting oxygen index respectively, and antibacterial test was carried out, compared with the flax fabrics treated with chitosan ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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PUM

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Abstract

The invention relates to a preparation method of a cellulose fabric having antibacterial and inflaming-retarding functions, belonging to the field of production of textiles. The preparation method comprises the following steps: dissolving chitosan phosphate into a butanetetracarboxylic acid solution, adding sodium hypophosphite having catalytic amount into the solution to prepare fabric treatment fluid, and dipping the cellulose fabric into the fabric treatment fluid, taking out and rolling for drying the fabric. According to the technical scheme, sodium hypophosphite is used as a catalyst, chitosan phosphate is dissolved into butanetetracarboxylic acid to be prepared into the fabric treatment fluid, and the cellulose fabric is dipped into the fabric treatment fluid, is taken out and is rolled to be dried, thus, the cellulose fabric has antibacterial and inflaming-retarding functions and has remarkable beneficial effects.

Description

technical field [0001] The invention relates to a preparation method of a cellulose fabric with antibacterial and flame-retardant functions, belonging to the field of textile production. Background technique [0002] The application fields of fabrics are extremely wide, such as clothing fabrics, decorative fabrics, automotive fabrics, industrial fabrics, medical fabrics and aerospace military fabrics, etc., which are widely used in various fields related to the national economy and people's livelihood. Due to the low thermal stability of cellulose fibers , at 300°C to 400°C, it can be dehydrated to produce aliphatic and depolymerized to produce levoglucosan and then pyrolyzed. Levoglucosan decomposition products have high flammability and low molecular weight, and the oxidation heat can support the further development of cellulose. Pyrolysis. [0003] Moreover, because the application of fabrics is closely related to people's daily life, and it is common for wearable produc...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M15/03D06M11/70D06M13/192D06M101/06
Inventor 韩晓建李发勇杨光道
Owner ANHUI AGRICULTURAL UNIVERSITY
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