Method for preparing rosa rugosa pollen from waste liquid of rosa rugosa subjected to essential oil extraction
A technology for rose pollen and roses, which is applied in the directions of food preparation, medical preparations containing active ingredients, pharmaceutical formulations, etc., can solve the problems of rose pollen and water resources waste, etc. The effect of increasing economic efficiency
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Embodiment 1
[0023] Example 1, the method for preparing rose pollen from the rose waste liquid after extracting essential oils is carried out according to the following steps: the first step is to take an appropriate amount of rose waste liquid after extracting essential oils to stand still, and after standing After the supernatant is separated, the mixed solution of the primary lower layer is obtained; in the second step, the mixed solution of the primary lower layer is left to stand, and after the supernatant is separated after standing, the mixed solution of the second lower layer is obtained; in the third step, the mixed solution of the second lower layer is obtained. After adding edible alcohol to the mixed liquid, adjust the pH to 9 to 11, then settle, and obtain pollen liquid after sedimentation; the fourth step, add deionized water to the pollen liquid and mix evenly to obtain a mixed liquid, and the mixed liquid is left to stand, After placing and separating the supernatant liqui...
Embodiment 2
[0024] Embodiment 2, as the optimization of the above-mentioned embodiment, the rose waste liquid after extracting the essential oil is obtained by the following method: collect fresh roses, add deionized water with 3 to 4 times the quality of fresh roses in the fresh roses, After heating to boiling, carry out reflux extraction while stirring, reflux extraction for 3h to 5h, the stirring rate is 150 rpm to 180 rpm, and the distillate after reflux extraction of essential oil is filtered through a 300 mesh to 500 mesh screen to obtain the extracted essential oil of rose waste. The container for reflux extraction can be a double-layer reflux reactor.
Embodiment 3
[0025] Example 3, as an optimization of the above example, in the first step, the time for standing the rose waste liquid after extracting the essential oil is 12h to 24h.
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