capsules and lithium-ion batteries
A lithium-ion battery, capsule technology, applied in secondary batteries, secondary battery repair/maintenance, circuits, etc., can solve problems such as safety performance impact and harsh working environment, and achieve the effect of improving safety performance
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Embodiment 1
[0029] (1) Preparation of capsules
[0030] Polyurea as the material of the capsule wall and propylene tricarbonate (PC) as the material of the capsule core were uniformly mixed by in-situ polymerization, acidified with NH4Cl as an acidic catalyst for 3 hours, and the final pH value was 2.0, and then styrene- Maleic anhydride was used as an emulsifier, continued to stir vigorously (rotation speed greater than 2000r / min), and then solidified at 70°C for 2 hours to obtain fluid spherical solid capsules with a median particle size of 100 μm and a wall thickness of 5 μm.
[0031] (2) Preparation of lithium-ion batteries
[0032]A Preparation of the positive pole piece: Mix the positive active material nickel cobalt lithium manganese oxide, the binder polyvinylidene fluoride (PVDF), the conductive agent conductive carbon black with the solvent N-methylpyrrolidone in a mass ratio of 90:5:5, A uniformly dispersed positive electrode slurry was obtained by high-speed stirring, and the...
Embodiment 2
[0037] (1) Preparation of capsules
[0038] Using the in-situ polymerization method, the polyamide as the material of the capsule wall and the propylene carbonate (PC) as the material of the capsule core are uniformly mixed, acidified with NH4Cl as an acidic catalyst for 4 hours, and the final pH value is 2.0, and then styrene-mass is added. Tonic anhydride was used as an emulsifier, and the mixture was continuously stirred vigorously (rotating speed greater than 2000r / min), and then solidified at 70°C for 2 hours to obtain fluid spherical solid capsules with a median particle size of 30 μm and a wall thickness of 0.5 μm.
[0039] (2) Preparation of lithium-ion batteries
[0040] Except that the capsule prepared in this example (i.e. Example 2) is used and the mass percentage of the capsule relative to the electrolyte solution is 20%, the rest is the same as Example 1.
Embodiment 3
[0042] (1) Preparation of capsules
[0043] Stir and mix the gelatin as the material of the capsule wall and the fluoropyridine as the material of the capsule core under the condition of 70°C / 3MPa, then add Span 80 and glutaraldehyde, continue to stir and mix evenly, and finally mix them at 30°C Cooling under the condition of / 3MPa, a fluid spherical solid capsule with a median particle size of 300 μm and a wall thickness of 50 μm was obtained.
[0044] (2) Preparation of lithium-ion batteries
[0045] Except that the capsule prepared in this example (i.e. Example 3) is used and the mass percentage of the capsule relative to the electrolyte solution is 30%, the rest is the same as that of Example 1.
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