Super-low density ceramic proppant and preparation method thereof
A technology of ultra-low density and proppant, which is applied in chemical instruments and methods, earthwork drilling, mining fluids, etc. It can solve the problems of high density and increase the difficulty of construction, achieve low density, improve the ability to resist crushing, and reduce density Effect
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[0023] The preparation method of the ultra-low density ceramsite proppant provided by the present invention comprises the following steps:
[0024] 1) Production of material A, wherein the ingredients contained in material A are bauxite, fly ash, clay and pore-enhancing agent, and the four ingredients are ground and mixed in proportion to obtain material A;
[0025] 2) Production of material B, wherein the ingredients contained in material B are bauxite, coal fly ash and manganese ore, and the three components are ground and mixed to obtain material B;
[0026] 3) Granulation, add material A into the pan-type ball forming machine, and add water to granulate by spraying method. When the particle size reaches the first particle size range, that is, the range of 0.1mm to 0.7mm, for example, it includes the following Specifications: 0.1-0.3mm, 0.1-0.4mm or 0.3-0.7mm. Gradually add material B during spraying and adding water. After the particle size reaches the second particle size...
Embodiment 1
[0034] Grind 2.5kg of bauxite, 3.0kg of fly ash, 4.0kg of clay, and 1.0kg of coal powder into a mixture with a particle size not greater than 325 mesh, and mix it evenly to form material A.
[0035] 7kg of bauxite, 2.5kg of fly ash and 0.5kg of manganese ore powder are ground into a mixture with a particle size not greater than 325 mesh, and mixed evenly to form B material.
[0036] Slowly add material A into the ball forming machine, add water to granulate by spraying method, control the particle size between 0.2mm and 0.4mm, then gradually add material B in the process of spraying and adding water, make the ball grow gradually, and control the particle size at 0.5mm Between mm ~ 0.9mm, the particles are dried and screened at 100 ~ 200 ° C, then enter the crucible, gradually increase the temperature in the muffle furnace, calcined at 1200-1250 ° C for 2.5 hours, after natural cooling, sieve according to particle size specifications A low-density proppant can be obtained. The...
Embodiment 2
[0038] Grind 2.5kg of bauxite, 2.5kg of fly ash, 5.0kg of clay, and 0.5kg of coal powder into a mixture with a particle size not greater than 325 mesh, and mix well to form material A.
[0039] 6kg of bauxite, 2.0kg of fly ash and 1.0kg of manganese ore powder are ground into a mixture with a particle size not greater than 325 mesh, and mixed evenly to form material B.
[0040] Slowly add material A into the ball forming machine, add water to granulate by spraying method, control the particle size between 0.3mm and 0.7mm, then gradually add material B in the process of spraying and adding water, make the ball grow gradually, and control the particle size at 0.5mm Between mm ~ 0.9mm, the particles are dried and screened at 100 ~ 200 ° C, then enter the crucible, gradually increase the temperature in the muffle furnace, calcined at 1200-1250 ° C for 2.5 hours, after natural cooling, sieve according to particle size specifications A low-density proppant can be obtained.
[0041]...
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