Plant type gas-phase copper corrosion inhibitor and preparation method thereof
A copper corrosion inhibitor, plant-based technology, applied in the field of plant-type gas-phase copper corrosion inhibitor and its preparation, can solve the problems of high toxicity, complex process of gas-phase copper corrosion inhibitor, difficult degradation, etc., achieve aromatic smell, increase corrosion resistance Corrosion effect and stability, the effect of simple preparation method
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preparation example Construction
[0027] The preparation method of vapor phase copper corrosion inhibitor provided by the invention comprises the following steps:
[0028] (1) crush the garlic, and ultrasonically mix it with an appropriate amount of medical alcohol, preferably in a weight ratio of 1:1; carry out solid-liquid separation and retain the liquid to obtain the garlic extract;
[0029] (2) Grind the fragrant leaves, and ultrasonically mix them with an appropriate amount of medical alcohol, preferably in a weight ratio of 1:5; carry out solid-liquid separation and retain the liquid to obtain the fragrant leaf extract;
[0030] (3) The garlic extract prepared in step (1) and the bay leaf extract prepared in step (2) were mixed according to a weight ratio of 3:1 to prepare the plant-type vapor phase copper corrosion inhibitor.
[0031] The volatile organic compounds in the garlic extract are identified by headspace mass spectrometry, and contain 30%-50% dipropenyl trisulfide, 10%-30% dipropenyl disulfid...
Embodiment 1
[0042] A plant-type vapor-phase copper corrosion inhibitor is obtained by compounding 75% of garlic extract and 25% of bay leaf extract according to weight percentage.
[0043] The plant-type gas-phase copper corrosion inhibitor is prepared as follows: according to the weight ratio, 1 part of garlic is mashed and evenly mixed with 1 part of 75% ethanol solution, and filtered after ultrasonic extraction to obtain milky yellow garlic extract; according to the weight ratio, the 1 part of bay leaf is cut into pieces and mixed evenly with 5 parts of 75% ethanol solution, filtered after ultrasonic extraction to obtain green bay leaf extract; the plant-type gas-phase copper corrosion inhibitor combines 75% of garlic extract with 25% of Prepared by uniformly mixing the bay leaf extract.
[0044] The main components and weight content of its volatile matter: 16.56% dipropenyl trisulfide, 7.43% dipropenyl disulfide, 7.24% 1-oxo-4,6-diazacyclooctane-5-thione, 31.61% eucalyptol, 15.3% L-...
Embodiment 2
[0050] The copper sheet added with the plant-type vapor-phase copper corrosion inhibitor in Example 1 and Comparative Examples 1 and 2 was subjected to atmospheric corrosion measurement.
[0051] According to the method in Comparative Example 3, the plant-type vapor-phase copper corrosion inhibitors described in Example 1 and Comparative Examples 1 and 2 were respectively placed in the covered vessel described in Comparative Example 3, and the airtight container was first dried at 35°C Middle pre-filming 24h, after pre-filming, other conditions are consistent with comparative example 3. Two days later, the atmospheric corrosion of the copper sheet was measured, and the results are shown in Table 1.
[0052] As can be seen from Table 1, the plant-type vapor-phase copper corrosion inhibitor described in Example 1 and Comparative Examples 1 and 2 all has a good corrosion inhibition effect, and the plant-type vapor-phase copper corrosion inhibitor described in Comparative Example ...
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