Preparation method of material with tobacco fragrance
A technology of aroma substances and tobacco extracts, which is applied in the field of preparation of tobacco aroma substances, can solve the problems of inability to fully obtain aroma substances in tobacco, waste of raw materials of aroma substances, and difficulty in large-scale production, so as to achieve rich and comprehensive aroma substances, increase Sugar and amino substance content, effects of avoiding changes and losses
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Embodiment 1
[0022] Tobacco leaves are dried and crushed and then extracted with 95% ethanol solution at 60°C for 4 hours. The ratio of tobacco raw materials to ethanol is 1:3 。 After solid-liquid separation, the filtrate was concentrated under reduced pressure to obtain tobacco extract A with a solid content of 55%, and the moisture content of the filter residue was adjusted to 60%, and 1% cellulase, 1% hemicellulase, 0.5% Pectinase was enzymatically hydrolyzed at 50°C for 4 hours, and after solid-liquid separation, the filtrate was concentrated under reduced pressure to obtain tobacco extract B with a solid content of 60%. Add proline with a mass percentage of 4% to extract B, and mix Heat at 100°C for 45 minutes to obtain tobacco reactant C, and mix tobacco extract A and tobacco reactant C at a ratio of 1:1 to obtain tobacco aroma substances.
[0023] Dilute the prepared tobacco aroma substance with 50% ethanol aqueous solution, spray it on the shredded tobacco at a dosage of 0.05%, adj...
Embodiment 2
[0025] Tobacco dust produced during the production of cigarettes is collected, dried and extracted with 70% ethanol solution at 80°C for 2 hours. The ratio of tobacco raw materials to ethanol is 1:4 。 After solid-liquid separation, the filtrate was concentrated under reduced pressure to obtain tobacco extract A with a solid content of 60%, and the moisture content of the filter residue was adjusted to 70%, and 0.5% cellulase, 0.5% hemicellulase, 0.5% Pectinase and 1% protease were hydrolyzed at 55°C for 6 hours, and after solid-liquid separation, the filtrate was concentrated under reduced pressure to obtain tobacco extract B with a solid content of 50%, and 2% hydrogen phosphate by mass was added to extract B Diammonia and 30% glycerol were mixed and heated at 90°C for 100 minutes to obtain tobacco reactant C. Tobacco extract A and tobacco reactant C were mixed at a ratio of 2:1 to obtain tobacco aroma substances.
[0026] After the prepared tobacco aroma substance is diluted...
Embodiment 3
[0028] Collect the fragments and tobacco stems produced during the cigarette production process, dry and pulverize them, and then extract them with 80% ethanol solution at 25°C for 48 hours. The ratio of tobacco raw materials to ethanol is 1:5 。 After solid-liquid separation, the filtrate was concentrated under reduced pressure to obtain tobacco extract A with a solid content of 50%, and the moisture content of the filter residue was adjusted to 75%, and 1.5% cellulase, 1.5% hemicellulase, 0.5% Pectinase and 2% protease were hydrolyzed at 55°C for 3 hours, and after solid-liquid separation, the filtrate was concentrated under reduced pressure to obtain tobacco extract B with a solid content of 70%, and 15% propylene glycol was added to the extract B, After mixing, heat at 110°C for 30 minutes to obtain tobacco reactant C, and mix tobacco extract A and tobacco reactant C at a ratio of 1:4 to obtain tobacco aroma substances.
[0029] The prepared tobacco aroma substance is dilut...
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