A method of degrading waste tires to oil
A technology for waste tires and waste oil, which is applied in the treatment of hydrocarbon oil, petroleum industry, hydrocarbon oil treatment products, etc., can solve problems such as the inability to meet cost control, reduce equipment requirements, reduce production costs, and eliminate the influence of harmful gases Effect
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Embodiment 1
[0023] A method for producing oil by degrading waste tires, comprising the following steps:
[0024] After the waste tires are cut into pieces in a cutting machine, they are added to the reactor with clarified lime water at a weight ratio of 1:10, and a desulfurizer is added to the reactor in an amount of clarified lime water 0.1 times of that, under nitrogen atmosphere, raise the temperature in the reactor to 400°C at a rate of 2°C / min, control the pressure to 16MPa, react at constant temperature and pressure for 1.1h, and then adjust the temperature to 200°C , keep the pressure constant for 10 minutes, then cool it down to normal temperature in 20s, and separate the gas-liquid products; mix tetrahydrofuran and desulfurizer according to the mass ratio of 3:0.1 and add them to the liquid phase, the addition amount is 10% of the mass of the liquid phase %, and it was ultrasonically treated for 20s, left to stand for 10min, oil and water were separated, and the oil phase was eva...
Embodiment 2
[0026] A method for producing oil by degrading waste tires, comprising the following steps:
[0027] After the waste tires are cut into pieces in a cutting machine, they are added to the reactor with clarified lime water at a weight ratio of 1:20, and a desulfurizer is added to the reactor in an amount of clarified lime water 0.4 times of that, under a nitrogen atmosphere, raise the temperature in the reactor to 450°C at a heating rate of 5°C / min, control the pressure to 18MPa, react at constant temperature and pressure for 3 hours, and then adjust the temperature to 270°C, Keep the pressure constant for 20 minutes, then cool it down to normal temperature in 40 seconds, and separate the gas and liquid products; mix tetrahydrofuran and desulfurizer according to the mass ratio of 3:0.5 and add it to the liquid phase, the amount added is 30% of the mass of the liquid phase , and it was ultrasonically treated for 30s, left to stand for 20min, oil and water were separated, and the ...
Embodiment 3
[0032] A method for producing oil by degrading waste tires, comprising the following steps:
[0033] After the waste tires are cut into pieces in a cutting machine, they are added to the reactor with clarified lime water at a weight ratio of 1:15, and a desulfurizer is added to the reactor in an amount of clarified lime water 0.3 times of that, under a nitrogen atmosphere, raise the temperature in the reactor to 430°C at a rate of 3°C / min, control the pressure to 17MPa, react at constant temperature and pressure for 2h, and then adjust the temperature to 250°C, Keep the pressure constant for 15 minutes, then cool it down to normal temperature in 30 seconds, and separate the gas and liquid products; mix tetrahydrofuran and desulfurizer according to the mass ratio of 3:0.3 and add it to the liquid phase, the amount added is 20% of the liquid phase mass , and it was treated with ultrasonic waves for 25s, left to stand for 15min, and the oil and water were separated, and the oil p...
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