A kind of high collapsible ceramic core and preparation method thereof
A ceramic core and collapsibility technology, applied in the field of materials, can solve the problems of no environmental protection core removal equipment, difficulty in core removal, etc., and achieve good sintering performance, good molding, and good collapsibility.
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preparation example Construction
[0050] A kind of preparation method of above-mentioned ceramic core, the step comprises:
[0051] 1) Mix and stir the quartz glass powder, mineralizer and binder according to the formula ratio; the state of the mixture can be sand;
[0052] 2) Dry the mixed material;
[0053] 3) Carry out ball milling after finishing;
[0054] 4) Prepare the ball-milled powder and the plasticizer in proportion to make a slurry;
[0055] 5) Press the slurry to form the core blank, the pressing pressure is 5-10 MPa; then send it into the roasting furnace for roasting, the roasting temperature is 500°C-800°C, and the roasting time is 240-360 minutes.
[0056] In the step 2), the material is dried in a vacuum environment, the ambient pressure is not greater than 0.08MPa, the ambient temperature is controlled at 30°C, and the temperature is kept for 120 minutes; in the step 3), the ball milling time is required to be 120-180 minutes.
example 1
[0058] a. In the quartz glass powder, the proportion of different particle size classifications is: 400 mesh accounts for 65%, 300 mesh accounts for 20%, 200 mesh accounts for 5%, and 150 mesh is the balance;
[0059] B, the consumption of described mineralizing agent is: the consumption of the corresponding mineralizing agent of every 1kg quartz glass powder is 5g;
[0060]c, the consumption of described binding agent is: the consumption of binding agent corresponding to every 1kg quartz glass powder is 100ml;
[0061] d. The dosage of the plasticizer is: 120 g of plasticizer per 1 kg of quartz glass powder; the mass percentage of polyethylene in the plasticizer is 16%.
[0062] In the step 5): the pressing pressure requirement is 6 MPa; the roasting temperature is 500°C for 60 minutes, the temperature is raised to 600°C for 30 minutes, the temperature is raised to 700°C for 30 minutes, and the temperature is raised to 800°C for 180 minutes;
example 2
[0064] a. In the quartz glass powder, the proportion of different particle size classifications is: 400 mesh accounts for 62%, 300 mesh accounts for 17%, 200 mesh accounts for 7%, and 150 mesh is the balance;
[0065] B, the consumption of described mineralizing agent is: the consumption of the corresponding mineralizing agent of every 1kg quartz glass powder is 8g;
[0066] c, the consumption of described binding agent is: the consumption of the binding agent corresponding to every 1kg quartz glass powder is 90ml;
[0067] d. The dosage of the plasticizer is: 140 g of plasticizer per 1 kg of quartz glass powder; the mass percentage of polyethylene in the plasticizer is 18%.
[0068] In the step 5): the pressing pressure requirement is 10 MPa; the roasting temperature is 500°C for 60 minutes, and the temperature is raised to 700°C for 300 minutes;
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