Dispersion method for carbon nanotubes

A carbon nanotube, dispersing technology, applied in mixing methods, chemical instruments and methods, dissolution and other directions, can solve the problems of the influence of agglomeration effect, the inability to obtain effective dispersion, the ineffective solution of carbon nanotubes, etc., to achieve obvious dispersion effect. Effect

Active Publication Date: 2016-05-04
QINGDAO UNIV OF SCI & TECH
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Problems solved by technology

However, the agglomeration effect of carbon nanotubes affects its excellent performance. At present, the main dispersion methods in the field of carbon nanotube research in my country include grinding, ultrasonic dispersion, and strong acid-base treatment, but these methods are limited to the laboratory research stage. The production of dispersed carbon nanotubes has not yet been effectively solved
Europe and the United States and other countries are ahead of us in research on carbo

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  • Dispersion method for carbon nanotubes

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[0017] The invention provides a carbon nanotube dispersion method that has obvious dispersion effect and can realize large-scale preparation. The first is to configure a mixture of carbon nanotubes and binder for dispersion, and the formula is a certain proportion of carbon nanotubes and binder. The nanomaterials and the binder are mixed in a certain ratio, and then the mixture is pressed into a certain shape of solid and semi-solid electrodes with mechanical pressure. The carbon nanotube mixture electrode is connected to one pole of the DC power supply (to connect with It is advisable to connect the negative pole of the power supply), and then the other pole of the power supply made of graphite, metal and other materials is kept at a certain distance from the electrode composed of carbon nanotube mixture. Turn on the power and the circuit to generate a certain intensity of electric heating sources such as arc, plasma, and electric spark between the two electrodes. The high tem...

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Abstract

The invention discloses a dispersion method for carbon nanotubes, belonging to the field of new materials. The method comprises the following steps: (1) mixing the carbon nanotubes with a binder; (2) pressing the obtained mixture so as to prepare an electrode; (3) connecting the electrode with a negative electrode of a direct-current power supply, and using materials like metal as a positive electrode of the power supply; (4) keeping a certain distance between the positive electrode and the negative electrode of the power supply; and (5) turning on the power supply so as to generate electro-induced heat sources like electric arcs, plasmas and electric sparks with a certain strength between the two electrodes of an electric circuit, and subjecting the binder absorbed by the carbon nanotubes to phase change under the action of high temperature so as to effectively disperse the carbon nanotubes. The invention has the following beneficial effects: the dispersion method for the carbon nanotubes provided by the invention has obvious dispersion effect and is easy to realize large-scale preparation.

Description

Technical field: [0001] The invention belongs to the field of new materials and relates to a method for dispersing carbon nanotubes. Background technique: [0002] Carbon nanotubes are tubular materials with nanometer-level diameters formed by curling graphite sheets at a certain helix angle. It has a very large aspect ratio, good heat exchange performance along the length direction, and low heat exchange performance in the vertical direction. Using its anisotropy and proper orientation, a composite material with superior thermal conductivity can be obtained . However, due to the strong van der Waals force between the carbon nanotubes, coupled with its very large aspect ratio, it is easy to agglomerate during production and use, thereby reducing its performance. In use, it is often necessary to fully disperse the agglomerates of carbon nanotubes to achieve the desired effect. [0003] The excellent properties of carbon nanotubes make it have a wide range of application prospects...

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Application Information

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IPC IPC(8): B01F3/12H01B13/00
CPCH01B13/00B01F23/51
Inventor 何燕李少龙朱圣坤薛浩浩
Owner QINGDAO UNIV OF SCI & TECH
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