A warm white phosphor excited by UV LEDs
A phosphor and warm white technology, applied in the field of rare earth luminescent materials, can solve the problems of poor stability, high cost and low excitation efficiency of phosphors
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Embodiment 1
[0033] Example 1: In 0.974 Dy 0.01 T m 0.01 Eu 0.006 NbO 4 Phosphor powder preparation
[0034] Weigh 0.9701g Nb 2 o 5 , 0.9869g In 2 o 3 , 0.0136g Dy 2 o 3 , 0.0141g Tm 2 o 3 and 0.0077g Eu, and ground it in an agate mortar for 15 minutes to mix the raw materials evenly. The mixed raw materials were placed in a corundum crucible, and the temperature was raised to 1000°C in a resistance furnace at a rate of 5°C / min for the first-stage sintering, and the sintering time was 12h. Then cool down with the furnace, grind the sintered product for 10 minutes, and then raise the temperature to 1250°C at a speed of 5°C / min for the second-stage sintering, and the sintering time is 24h. Grinding after cooling in the furnace, the composition can be obtained as In 0.98 Dy 0.01 T m 0.01 NbO 4 of fluorescent powder.
Embodiment 2
[0035] Example 2: In 0.98 Dy 0.01 T m 0.01 NbO 4 Phosphor powder preparation
[0036] Weigh 0.9701g Nb 2 o 5 , 0.9930g In 2 o 3 , 0.0136g Dy 2 o 3 and 0.0141g Tm 2 o 3 , the rest of the steps are the same as in Example 1.
Embodiment 3
[0037] Example 3: In 0.97 Dy 0.01 T m 0.01 Eu 0.01 NbO 4 Phosphor powder preparation
[0038] Weigh 0.9701g Nb 2 o 5 , 0.9869g In 2 o 3 , 0.0136g Dy 2 o 3 , 0.0141g Tm 2 o 3 And 0.0128g Eu, all the other steps are identical with embodiment 1.
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