Preparation of spongy activated carbon organic composite material for oil absorption and decontamination
A composite material, activated carbon technology, applied in the fields of adsorption water/sewage treatment, grease/oily substance/float removal device, and other chemical processes, etc. The effect of good oil absorption and decontamination performance
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Embodiment 1
[0027] (1) First, add about 10g of polyvinyl alcohol to 120mL of water to swell.
[0028] (2) Place (1) in a heat-collecting constant temperature magnetic stirrer at 95°C and stir slowly until it is completely dissolved.
[0029] (3) Cool down (2) to 70°C, add 9g of soluble starch and 15g of activated carbon dissolved in 20mL of water, and mix well.
[0030] (4) Add 32mL of 9% dilute sulfuric acid solution and 12mL of 40% formaldehyde solution, and stir well.
[0031] (5) Place in a constant temperature water bath at 70°C for acetalization reaction to obtain activated carbon / organic composite three-dimensional network pore structure material.
[0032] (6) Place (5) in n-hexane for solvent replacement.
[0033] (7) Take (6) out of n-hexane and fully dry it to obtain the finished activated carbon / organic composite three-dimensional network pore structure material.
Embodiment 2
[0035] (1) First, add about 10g of polyvinyl alcohol to 140mL of water to swell.
[0036] (2) Place (1) in a heat-collecting constant temperature magnetic stirrer at 95°C and stir slowly until it is completely dissolved.
[0037] (3) Cool down (2) to 70°C, add 10g of soluble starch and 10g of activated carbon dissolved in 20mL of water, and mix well.
[0038] (4) Add 32mL of 9% dilute sulfuric acid solution and 8mL of 40% formaldehyde solution, and stir well.
[0039] (5) Place in a constant temperature water bath at 55°C for acetalization reaction to obtain activated carbon / organic composite three-dimensional network pore structure material.
[0040] (6) Place (5) in n-hexane for solvent replacement.
[0041] (7) Take (6) out of n-hexane and fully dry it to obtain the finished activated carbon / organic composite three-dimensional network pore structure material.
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