Multipurpose spray glue and preparation method thereof
A multi-purpose, glue-spraying technology, applied in adhesives, adhesive additives, non-polymer organic compound adhesives, etc., can solve problems such as low adhesion, strong penetration, and easy corrosion, and achieve strong adhesion , the effect of low penetration
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specific Embodiment 1
[0033] The weight components of multi-purpose spray glue are as follows:
[0034] SBR rubber (SBR1712): 7 parts;
[0035] Dimethyl carbonate: 38 parts;
[0036] Disproportionated rosin: 14 parts;
[0037] Ethyl acetate: 20 parts;
[0038] C 5 Petroleum resin: 3 parts;
[0039] Polyvinyl alcohol with a number average molecular weight of 16000-20000: 1 part by weight;
[0040] Hydroxyethyl methacrylate: 5 parts by weight;
[0041] Butane: 18 parts.
[0042] The preparation method is:
[0043] Step 1: First add dimethyl carbonate and ethyl acetate into the reaction kettle;
[0044] Step 2: Add SBR rubber, tackifying resin, and disproportionated rosin to the reactor, and stir for 1 hour at room temperature;
[0045] Step 3: Add polyvinyl alcohol and hydroxyethyl methacrylate to the reactor, pressurize it to 0.3MPa (gauge pressure), and react at 65°C for 0.5h;
[0046] Step 4: Cool the reaction kettle to normal temperature and keep it at normal pressure and stir for 2h;
[0047] Step 5: Filter the re...
specific Embodiment 2
[0048] The weight components of multipurpose spray glue are as follows:
[0049] SBR rubber (SBR1712): 9 parts;
[0050] Dimethyl carbonate: 33 parts;
[0051] Disproportionated rosin: 16 parts;
[0052] Ethyl acetate: 22 parts;
[0053] C 9 Petroleum resin: 2 parts;
[0054] Polyvinyl alcohol with a number average molecular weight of 16000-20000: 2 parts by weight;
[0055] Hydroxyethyl methacrylate: 31 parts by weight;
[0056] Butane: 16 parts.
[0057] The preparation method is: Step 1: First add dimethyl carbonate and ethyl acetate to the reaction kettle;
[0058] Step 2: Add SBR rubber, tackifier resin, and disproportionated rosin to the reactor, and stir for 1.5h at room temperature;
[0059] Step 3: Add polyvinyl alcohol and hydroxyethyl methacrylate to the reactor, pressurize it to 0.5MPa (gauge pressure), and react at 60°C for 0.5h;
[0060] Step 4: Cool the reactor to normal temperature and keep it under normal pressure and stir for 1 hour;
[0061] Step 5: Filter the reaction produc...
specific Embodiment 3
[0062] The weight components of multi-purpose spray glue are as follows:
[0063] SBR rubber (SBR1500): 8 parts;
[0064] Dimethyl carbonate: 35 parts;
[0065] Disproportionated rosin: 15 parts;
[0066] Ethyl acetate: 21 parts;
[0067] Terpene resin: 2.5 parts;
[0068] Polyvinyl alcohol with a number average molecular weight of 16000-20000: 1.5 parts by weight;
[0069] Hydroxyethyl methacrylate: 4 parts by weight;
[0070] Butane: 17.5 parts.
[0071] The preparation method is specifically:
[0072] Step 1: First add dimethyl carbonate and ethyl acetate into the reaction kettle;
[0073] Step 2: Add SBR rubber, tackifying resin, and disproportionated rosin to the reactor, and stir for 1.2h at room temperature;
[0074] Step 3: Add polyvinyl alcohol and hydroxyethyl methacrylate to the reactor, pressurize it to 0.4MPa (gauge pressure), and react at 62°C for 0.8h;
[0075] Step 4: Cool down the reactor to normal temperature and keep it under normal pressure and stir for 1.5h;
[0076] Step 5:...
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