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Oil-water separation device and method for simultaneously extracting light volatile oil and heavy volatile oil

An oil-water separation device and a technology for volatile oil, which are applied in the directions of essential oils/spices, fat generation, etc., can solve the problems of large volume, small heat exchange area of ​​condenser, heat exchange efficiency, inability to collect volatile oil, etc., and achieve simple extraction method and volatile oil collection. high volume effect

Inactive Publication Date: 2016-10-12
CHONGQING TAIJI INDAL GROUP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the process of volatile oil extraction, the oil-water separation system of the multi-energy tank is generally used, but the heat exchange area of ​​the condenser in the existing multi-energy tank oil-water separation system is generally small (generally 6m 3 The tank is only less than 3m 2 ), the tube wall of the condenser is too thick, which seriously affects the heat exchange efficiency, and the main condenser is horizontally placed, which affects the rapid replacement of oil-water condensate; the rising pipe from the evaporator to the main condenser has no heat preservation and condensate with slight pressure The impact on the oil-water liquid level of the oil-water separator leads to low collection efficiency of light and heavy volatile oils, and it is even impossible to collect volatile oils containing only heavy oil or heavy oil medicinal materials
But in essence, this does not fundamentally solve the problem of simultaneous extraction of light and heavy volatile oils
Moreover, the method of "collecting aromatic water" is bulky, and tons of aromatic water have problems in storage, transshipment, pollution prevention, and deterioration.

Method used

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  • Oil-water separation device and method for simultaneously extracting light volatile oil and heavy volatile oil
  • Oil-water separation device and method for simultaneously extracting light volatile oil and heavy volatile oil
  • Oil-water separation device and method for simultaneously extracting light volatile oil and heavy volatile oil

Examples

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Effect test

Embodiment 1

[0026] An oil-water separation device that can extract light volatile oil and heavy volatile oil at the same time, the structure is as follows figure 1 shown. Including extraction tank 1, condenser 2 and volatile oil separator 3, the top of the condenser 2 is open and installed vertically or inclined at an angle greater than 50° with the horizontal direction, the bottom of the condenser 2 is provided with a steam inlet and a condensate outlet , the steam inlet of the condenser 2 is connected to the steam outlet of the extraction tank 1 through a pipeline 4 with an insulating layer, and the condensate outlet of the condenser 2 is connected to the volatile oil separator 3; the upper part of the volatile oil separator 3 is provided with The capture agent adder 5 and the volatile oil outlet 6 controlled by the oil collection valve.

[0027]In the present invention, the upper ends of the condenser 2 and the volatile oil separator 3 are emptied to keep the liquid level of the evapo...

Embodiment 2

[0039] The method of extracting light volatile oil and heavy volatile oil simultaneously by using an oil-water separation device that can simultaneously extract light volatile oil and heavy volatile oil, the specific steps are as follows (in this embodiment, taking the 5 flavors of oil extracting medicinal materials of sinusitis oral liquid as an example, Magnolia magnolia, Schizonepeta, Peppermint, Bamboo Leaf Bupleurum).

[0040] Add the 4 flavors of sinusitis oral liquid to extract oil medicinal materials (1% prescription amount) into the extraction tank for 5 hours, and add 300ml 60-90°C petroleum ether from the capture agent adder of the volatile oil separator as a capture agent, and keep the condensate The temperature of dripping into the oil receiver does not exceed 30°C, after letting go of the water layer, finally collect the mixed liquid in the upper oil layer and measure it. Transfer the oil layer mixture of volatile oil and petroleum ether into a 2L rotary evaporat...

Embodiment 3

[0050] The method for simultaneously extracting light volatile oil and heavy volatile oil by using an oil-water separation device capable of simultaneously extracting light volatile oil and heavy volatile oil, the specific steps are as follows:

[0051] 40Kg of the medicinal material Angelica sinensis that only blindly contains both heavy oil and light oil in the Guiqi Shengxue granule is put into 500L existing crude oil water separation device without multi-energy tank transformation (its structure is as follows: image 3 Shown) carried out co-water distillation to extract Angelica volatile oil for 5 hours. The results showed that no volatile oil could be collected, only microemulsion turbid distilled water could be collected, and three consecutive batches of tests could not collect a little volatile oil.

[0052] The oil-water separation device of the present invention was carried out three batches of tests according to the method of Example 2, and the results are shown in T...

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Abstract

The invention discloses an oil-water separation device and method for simultaneously extracting light volatile oil and heavy volatile oil. The device comprises an extraction tank, a condenser and a volatile oil separator. The condenser can be vertically or obliquely mounted, the top of the condenser is emptied, and the part between the extraction tank and the condenser is subjected to heat preservation setting, so that the problem that the conventional volatile oil extracting device is relatively low in volatile oil collecting amount and cannot collect heavy volatile oil or collect light volatile oil and heavy volatile oil at the same time; the method for extracting light volatile oil and heavy volatile oil by utilizing the device is further disclosed, is simple, and high in volatile oil collecting amount, can use four types of organic solvents as trapping agents, is safe and non-toxic, and can quickly extract light volatile oil and heavy volatile oil at the same time.

Description

technical field [0001] The invention belongs to the field of volatile oil refining, and in particular relates to an oil-water separation device capable of simultaneously extracting light volatile oil and heavy volatile oil, and also relates to a method for simultaneously extracting light volatile oil and heavy volatile oil by using the device. Background technique [0002] Volatile oil, also known as aromatic oil, is a common sesquiterpene compound in plant tissues, which is extremely difficult to dissolve in water, but the aqueous solution of trace volatile oil at PPM level has a strong aromatic smell, so it is also called aromatic water. According to the relative density of volatile oil and water, the relative density lower than water is called "light oil"; the relative density higher than water is called "heavy oil". In the process of volatile oil extraction, the oil-water separation system of the multi-energy tank is generally used, but the heat exchange area of ​​the co...

Claims

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Application Information

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IPC IPC(8): C11B9/02
CPCC11B9/027C11B9/022
Inventor 白礼西冯天炯官柳刘超王文成胡彬程地英吴用彦邓大用汤加兵
Owner CHONGQING TAIJI INDAL GROUP
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