Oil-water separation device and method for simultaneously extracting light volatile oil and heavy volatile oil
An oil-water separation device and a technology for volatile oil, which are applied in the directions of essential oils/spices, fat generation, etc., can solve the problems of large volume, small heat exchange area of condenser, heat exchange efficiency, inability to collect volatile oil, etc., and achieve simple extraction method and volatile oil collection. high volume effect
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Embodiment 1
[0026] An oil-water separation device that can extract light volatile oil and heavy volatile oil at the same time, the structure is as follows figure 1 shown. Including extraction tank 1, condenser 2 and volatile oil separator 3, the top of the condenser 2 is open and installed vertically or inclined at an angle greater than 50° with the horizontal direction, the bottom of the condenser 2 is provided with a steam inlet and a condensate outlet , the steam inlet of the condenser 2 is connected to the steam outlet of the extraction tank 1 through a pipeline 4 with an insulating layer, and the condensate outlet of the condenser 2 is connected to the volatile oil separator 3; the upper part of the volatile oil separator 3 is provided with The capture agent adder 5 and the volatile oil outlet 6 controlled by the oil collection valve.
[0027]In the present invention, the upper ends of the condenser 2 and the volatile oil separator 3 are emptied to keep the liquid level of the evapo...
Embodiment 2
[0039] The method of extracting light volatile oil and heavy volatile oil simultaneously by using an oil-water separation device that can simultaneously extract light volatile oil and heavy volatile oil, the specific steps are as follows (in this embodiment, taking the 5 flavors of oil extracting medicinal materials of sinusitis oral liquid as an example, Magnolia magnolia, Schizonepeta, Peppermint, Bamboo Leaf Bupleurum).
[0040] Add the 4 flavors of sinusitis oral liquid to extract oil medicinal materials (1% prescription amount) into the extraction tank for 5 hours, and add 300ml 60-90°C petroleum ether from the capture agent adder of the volatile oil separator as a capture agent, and keep the condensate The temperature of dripping into the oil receiver does not exceed 30°C, after letting go of the water layer, finally collect the mixed liquid in the upper oil layer and measure it. Transfer the oil layer mixture of volatile oil and petroleum ether into a 2L rotary evaporat...
Embodiment 3
[0050] The method for simultaneously extracting light volatile oil and heavy volatile oil by using an oil-water separation device capable of simultaneously extracting light volatile oil and heavy volatile oil, the specific steps are as follows:
[0051] 40Kg of the medicinal material Angelica sinensis that only blindly contains both heavy oil and light oil in the Guiqi Shengxue granule is put into 500L existing crude oil water separation device without multi-energy tank transformation (its structure is as follows: image 3 Shown) carried out co-water distillation to extract Angelica volatile oil for 5 hours. The results showed that no volatile oil could be collected, only microemulsion turbid distilled water could be collected, and three consecutive batches of tests could not collect a little volatile oil.
[0052] The oil-water separation device of the present invention was carried out three batches of tests according to the method of Example 2, and the results are shown in T...
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