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Wet spinning technology applicable to preparing livistona chinensis leaf cellulose regenerated fiber

A cellulose regeneration, wet spinning technology, applied in the cellulose solution of artificial filament, wet spinning, spinning solution preparation and other directions, can solve the problem of no report, no discovery, etc. question

Inactive Publication Date: 2016-11-09
WUYI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Palm leaf cellulose regenerated fiber meets the needs of modern people's production and life, but in daily life, such products have not been found, and the literature related to the process of preparing palm leaf cellulose regenerated fiber has not been reported.

Method used

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  • Wet spinning technology applicable to preparing livistona chinensis leaf cellulose regenerated fiber

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] A preparation of palm leaf cellulose spinning solution: a. Dissolve 800 grams of anhydrous lithium chloride solid in dimethylacetamide solvent at a ratio of 80 grams per liter of anhydrous lithium chloride solid to make anhydrous chlorine Lithium chloride / dimethylacetamide mixed solvent 10 liters; Press the ratio of palm leaf cellulose 60 grams per liter, 600 grams of palm leaf cellulose are dissolved in 10 liters of mixed solvents that step a makes, make spinning dope 10 liters;

[0019] B wet spinning: pour 10 liters of spinning solution prepared in step A into the liquid storage tank of the wet spinning machine, heat the liquid storage tank of the wet spinning machine to 65 ° C, and wait for spinning in the liquid storage tank After the temperature of the silk liquid reaches equilibrium and stability: ①The spinning liquid passes through the metering pump and filter, and is sprayed out from the spinneret; ②The spinning liquid sprayed out from the spinneret is directly...

Embodiment 2

[0022] A preparation of palm leaf cellulose spinning solution: a. Dissolve 800 grams of anhydrous lithium chloride solid in dimethylacetamide solvent at a ratio of 80 grams per liter of anhydrous lithium chloride solid to make anhydrous chlorine Lithium chloride / dimethylacetamide mixed solvent 10 liters; Press the ratio of palm leaf cellulose 60 grams per liter, 600 grams of palm leaf cellulose are dissolved in 10 liters of mixed solvents that step a makes, make spinning dope 10 liters;

[0023] B wet spinning: pour 10 liters of spinning solution prepared in step A into the liquid storage tank of the wet spinning machine, heat the liquid storage tank of the wet spinning machine to 95 °C, and wait for spinning in the liquid storage tank After the temperature of the silk liquid reaches equilibrium and stability: ①The spinning liquid passes through the metering pump and filter, and is sprayed out from the spinneret; ②The spinning liquid sprayed out from the spinneret is directly ...

Embodiment 3

[0026] A preparation of palm leaf cellulose spinning solution: a. Dissolve 800 grams of anhydrous lithium chloride solid in dimethylacetamide solvent at a ratio of 80 grams per liter of anhydrous lithium chloride solid to make anhydrous chlorine Lithium chloride / dimethylacetamide mixed solvent 10 liters; Press the ratio of palm leaf cellulose 60 grams per liter, 600 grams of palm leaf cellulose are dissolved in 10 liters of mixed solvents that step a makes, make spinning dope 10 liters;

[0027] B wet spinning: pour 10 liters of spinning solution prepared in step A into the liquid storage tank of the wet spinning machine, heat the liquid storage tank of the wet spinning machine to 35 ° C, and spin in the liquid storage tank After the temperature of the silk liquid reaches equilibrium and stability: ①The spinning liquid passes through the metering pump and filter, and is sprayed out from the spinneret; ②The spinning liquid sprayed out from the spinneret is directly added to the...

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Abstract

The invention relates to a wet spinning technology applicable to preparing livistona chinensis cellulose regenerated fiber. The technology comprises preparation of a spinning solution obtained by dissolving livistona chinensis leaf cellulose regenerated fiber into an anhydrous lithium chloride / dimethylacetamide mixed solvent and wet spinning technology performed within the condition range; the spinning solution temperature of 35-95 DEG C, the coagulating bath temperature if 15-45 DEG C, the dimethylacetamide volume concentration in a coagulating bath is 0-30%, the temperature of a stretch bath is 30-60 DEG C, and the stretching ratio is 1.2-1.8 times. The livistona chinensis cellulose regenerated fiber prepared through the wet spinning technology within the condition range has the good mechanical property and moisture regain, and the livistona chinensis cellulose regenerated fiber will become novel cellulose regenerated fiber.

Description

technical field [0001] The invention relates to a wet spinning process after dissolving palm leaf cellulose with anhydrous lithium chloride / dimethylacetamide solvent system, belongs to the technical field of plant regenerated fiber, in particular to a kind of process suitable for preparing palm leaf cellulose Wet spinning process of regenerated fiber. Background technique [0002] In the textile industry, cellulose regenerated fiber has always been valued by people because of its rich resources, environmental friendliness, and comfortable products. Although its consumption proportion is not as high as that of synthetic fibers in recent years, due to the increasing depletion of coal and oil, and the serious "white pollution" caused by the non-degradable waste of synthetic fiber products is becoming more and more serious, and restricted by the area of ​​cultivated land, the output of virgin fibers It is also subject to certain restrictions, and the demand for fiber is constan...

Claims

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Application Information

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IPC IPC(8): D01D5/06D01D1/02D01D5/14D01F2/02
CPCD01D5/06D01D1/02D01D5/14D01F2/02
Inventor 贾永堂聂伟利于晖黄钢董凤春曾显华
Owner WUYI UNIV
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