A kind of preparation method of alumina type catalyst of disproportionation methyltrichlorosilane reaction
A disproportionation methyltrichlorosilane and catalyst technology, which is applied in the field of alumina catalyst preparation, can solve the problems of easy loss of AlCl3, achieve the effects of solving environmental pollution and safety problems, improving efficiency, and reducing production costs
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0037] This embodiment will illustrate that the inventive method is 1:2 with double salt Al / Na ratio, double salt (NaAlCl 4 ) loading at 9%, the selected Al 2 o 3 α-Al 2 o 3 , according to the reaction path of high temperature and high pressure load combined with impregnation method.
[0038] With 9% double salt load and 1:2 Al / Na ratio, weigh a certain amount of NaCl and AlCl 3 , and dissolve NaCl in water to form a solution, and weigh 4g α-Al 2 o 3 The carrier was impregnated in NaCl solution for 1 h, and then dried in a muffle furnace at 150 °C. After drying, AlCl was added to it 3 Transfer the reaction system to a polytetrafluoroethylene rod and seal it, and place it in a muffle furnace at 220°C for 16 hours; after the reaction is complete, cool it slowly at room temperature to obtain the modified Al 2 o 3 type catalyst.
[0039] The efficiency of producing dimethyldichlorosilane by the disproportionation reaction of the alumina catalyst prepared in this example t...
Embodiment 2
[0041] This embodiment will illustrate that the inventive method is 1:2 with double salt Al / Na ratio, double salt (NaAlCl 4 ) loading at 12%, the selected Al 2 o 3 α-Al 2 o 3 , according to the reaction path of high temperature and high pressure load combined with impregnation method.
[0042] With 12% double salt load and 1:2 Al / Na ratio, weigh a certain amount of NaCl and AlCl 3 , and dissolve NaCl in water to form a solution, and weigh 4g α-Al 2 o 3 The carrier was impregnated in NaCl solution for 1 h, and then dried in a muffle furnace at 150 °C. After drying, AlCl was added to it 3 Transfer the reaction system to a polytetrafluoroethylene rod and seal it, and place it in a muffle furnace at 220°C for 16 hours; after the reaction is complete, cool it slowly at room temperature to obtain the modified Al 2 o 3 type catalyst.
[0043] The efficiency of producing dimethyldichlorosilane by the disproportionation reaction of the alumina catalyst prepared in this example...
Embodiment 3
[0045] This embodiment will illustrate that the inventive method is 1:2 with double salt Al / Na ratio, double salt (NaAlCl 4 ) loading at 12%, the selected Al 2 o 3 β-Al 2 o 3 , according to the reaction path of high temperature and high pressure load combined with impregnation method.
[0046] With 12% double salt load and 1:2 Al / Na ratio, weigh a certain amount of NaCl and AlCl 3 , and dissolve NaCl in water to form a solution, and then weigh 4gβ-Al 2 o 3 The carrier was impregnated in NaCl solution for 1 h, and then dried in a muffle furnace at 150 °C. After drying, AlCl was added to it 3 Transfer the reaction system to a polytetrafluoroethylene rod and seal it, and place it in a muffle furnace at 220°C for 16 hours; after the reaction is complete, cool it slowly at room temperature to obtain the modified Al 2 o 3 type catalyst.
[0047] The efficiency of producing dimethyldichlorosilane by the disproportionation reaction of the alumina catalyst prepared in this exa...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More