Preparation method of fiber with humidifying function
A technology of functional fibers and humidity control, which is applied in the field of preparation of humidity control functional fibers, can solve the problems affecting comfort, etc., and achieve the effects of long aging, good dispersion and enhanced fiber strength
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Embodiment 1
[0017] A preparation method for humidity-regulating functional fibers, which is carried out in the following steps:
[0018] Step 1: Prepare gamma-cyclodextrin as a gamma-cyclodextrin solution with a mass concentration of 5%, add silver nitrate whose mass is 0.4 times that of gamma-cyclodextrin to the gamma-cyclodextrin solution, stir evenly, Control the pH value of the solution at 5, heat it to 55°C and keep it warm for 2.5 hours under the condition of avoiding light, then centrifuge to obtain the solid, wash and dry the solid, dissolve it in the sodium hydroxide solution, and add it to the sodium hydroxide solution Add sodium borohydride with a mass of 1% solid to adjust the pH to 7.5, then stir, centrifuge again and dry to prepare the silver-loaded γ-cyclodextrin.
[0019] Step 2: Prepare cellulose and silk fibroin as a mixed solution with a mass concentration of cellulose of 3% and a mass concentration of silk fibroin of 2%, and successively add silver-loaded γ-cyclopaste ...
Embodiment 2
[0023] A preparation method for humidity-regulating functional fibers, which is carried out in the following steps:
[0024] Step 1: Prepare gamma-cyclodextrin as a gamma-cyclodextrin solution with a mass concentration of 4%, add silver nitrate whose mass is 0.3 times that of gamma-cyclodextrin to the gamma-cyclodextrin solution, stir evenly, Control the pH value of the solution at 4, heat to 50°C and keep it warm for 3 hours under the condition of avoiding light, and then centrifuge to obtain a solid, wash and dry the solid, dissolve it in sodium hydroxide solution, and add it to the sodium hydroxide solution Adding 0.5% sodium borohydride with a mass of solid, adjusting the pH to 7, then stirring, centrifuging again and drying to prepare the silver-loaded γ-cyclodextrin.
[0025] Step 2: Prepare cellulose and silk fibroin as a mixed solution with a mass concentration of cellulose of 2% and a mass concentration of silk fibroin of 1%, and add silver-loaded γ-cyclopaste with a ...
Embodiment 3
[0029] A preparation method for humidity-regulating functional fibers, which is carried out in the following steps:
[0030] Step 1: Prepare gamma-cyclodextrin as a gamma-cyclodextrin solution with a mass concentration of 6%, add silver nitrate whose mass is 0.5 times that of gamma-cyclodextrin to the gamma-cyclodextrin solution, stir evenly, Control the pH value of the solution at 6, heat it to 60°C and keep it warm for 2 hours under the condition of avoiding light, then centrifuge to obtain a solid, wash and dry the solid, dissolve it in sodium hydroxide solution, and add it to the sodium hydroxide solution Adding 1.5% sodium borohydride with a mass of solid, adjusting the pH to 8, then stirring, centrifuging again and drying to prepare the silver-loaded γ-cyclodextrin.
[0031] Step 2: Prepare cellulose and silk fibroin as a mixed solution with a mass concentration of cellulose of 4% and a mass concentration of silk fibroin of 3%, and add silver-loaded γ-cyclopaste with a m...
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