Negative electrode for secondary battery and manufacturing method of the same
A secondary battery and negative electrode technology, applied in the field of secondary battery negative electrode and its preparation, can solve the problems of reduced electrode density, decreased unit volume capacity, large specific surface area, etc., to achieve improved charging capacity, high electrode density, excellent electrolysis The effect of liquid immersion
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[0101] The present invention can provide a method for preparing a negative electrode for a secondary battery. The method for preparing a negative electrode for a secondary battery includes: step (a), preparing a slurry solution containing Si-block copolymer core-shell particles and a carbonaceous raw material mixed therewith The mixture; Step (b), heat-treating the above-mentioned mixture; Step (c), preparing a carbon-silicon composite by pulverizing the above-mentioned mixture after performing a carbonization process on the heat-treated above-mentioned mixture; Step (d), mixing the above-mentioned carbon-silicon Composite and graphite to prepare negative electrode active material; and step (e), coating above-mentioned negative electrode active material, conductive material, binding material and thickening agent on current collector, the carbonization and pulverization in above-mentioned step (c) are carried out at least repeatedly 2 times, in the particle distribution in the n...
Embodiment 1
[0145] Polyacrylate and polystyrene were synthesized into polyacrylate-polystyrene block copolymers by a reversible addition fragmentation chain transfer method. At this point, the average molecular weight (M n ) is 4090g / mol, the average molecular weight of polystyrene (M n ) is 29370 g / mol. 0.1 g of polyacrylate-polystyrene block copolymer and 8.9 g of N-methyl-2-pyrrolidone dispersion medium were mixed. 1 g of Si particles having an average particle diameter of 50 nm was added to 9 g of the mixed solution. The solution added with Si particles was treated with ultrasonic waves at 20 kHz for 10 minutes and paused for 20 minutes by means of a sonic horn, thereby preparing a mixture containing Si-block copolymer core-shell particles.
[0146] The above mixture and amorphous carbon evaporated at a temperature of 350° C. were mixed and stirred for about 30 minutes, thereby preparing a mixture in which amorphous carbon was dissolved in an N-methyl-2-pyrrolidone dispersion mediu...
Embodiment 2
[0151] A negative electrode active material was prepared by the same method as in Example 1 except that the D50 of spherical graphite was 14 μm.
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